Download Inertsilシリーズ 14φ分取カラム発売のお知らせ

Transcript
㪠㫅㪼㫉㫋㫊㫀㫃㩷㪈㪋㩷㫄㫄㩷㪠㪅㪛㪅㩷ಽข䉦䊤䊛
Inertsil 14 mm I.D. ಽข䉦䊤䊛
㪩
ౝᓘ㪈㪋㩷㫄㫄䈱ᣂ䈢䈭ಽข䉦䊤䊛䈏⊒ᄁ䈘䉏䉁䈚䈢䇯
᳢↪㪟㪧㪣㪚䉕↪䈇䇮ᄢ㊂䈮ಽข䈜䉎㓙䈮᦭ല䈭ಽข䉦䊤䊛䈪䈜䇯
䈜䇯
⹜ᢱ⽶⩄㊂䋲୚
᳢↪㪟㪧㪣㪚䈪ಽข䉕ⴕ䈉㓙䈮૶↪䈜䉎䉦䊤䊛䈲䇮ౝᓘ㪈㪇㩷㫄㫄䈱ಽข䉦䊤䊛䈏ਥᵹ䈪䈜䇯ᣂ⵾ຠ䈱ౝᓘ
㪈㪋㩷㫄㫄䈱ಽข䉦䊤䊛䉕૶↪䈜䉎䈫䇮ౝᓘ㪈㪇㩷㫄㫄䈱䉦䊤䊛䈮Ყ䈼䇮䋲୚䈱䉰䊮䊒䊦䉕৻ᐲ䈮ಽขน⢻䈪䈜䇯
㪋㩷㫄㫄䈱ಽข䉦䊤䊛䉕૶↪䈜䉎䈫䇮ౝᓘ㪈㪇㩷㫄㫄䈱䉦䊤䊛䈮Ყ䈼䇮䋲୚䈱䉰䊮䊒䊦䉕৻ᐲ䈮ಽขน⢻䈪䈜䇯
ᢿ㕙Ⓧߣࠨࡦࡊ࡞⽶⩄㊂
ౝᓘOOߩಽขࠞ࡜ࡓ㧔ᦨㆡᵹ㊂O.OKP
ࠞ࡜ࡓᢿ㕙ⓍߦᲧ଀ߒߡࠨࡦࡊ࡞⽶⩄㊂߇Ⴧടߒ߹ߔ‫ޕ‬
߹ߚ‫ޔ‬ᢿ㕙ⓍߦᲧ଀ߒߡᵹㅦࠍ਄ߍࠆߣหߓಽ㔌߇ᓧࠄࠇ
߹ߔ‫ޕ‬
GZ
OI⹜ᢱ⽶⩄
ౝᓘOOߩࠞ࡜ࡓߪ
ౝᓘOOߩࠞ࡜ࡓߣᲧߴߡ
ౝᓘOOߩಽขࠞ࡜ࡓ
ᦨㆡᵹ㊂O.OKP㧕
⚂㧞୚ߦࠨࡦࡊ࡞⽶⩄㊂߇
Ⴧടߒ߹ߔ‫ޕ‬
GZ
OI⹜ᢱ⽶⩄
㶎૶↪ⅣႺ䈮䉋䈦䈩䈲ᬌ಴ེ䈱䉶䊦䈏⎕៊䈜䉎႐ว
㩷㩷㩷 䈏䈅䉎䈢䉄䇮಴ญ㈩▤䈱⢛࿶䈮䈲䈗ᵈᗧ䈒䈣䈘䈇䇯
㩷㩷㩷㩷㩷㩷
䇭లႯ೷䈱⒳㘃䈏⼾ን䇭䇭
లႯ೷
೷䈱⒳㘃䈏⼾ን䇭䇭䇭䇭
㪠㫅㪼㫉㫋㫊㫀㫃㩷㪦㪛㪪㪄㪊䉇㪦㪛㪪㪄㪋䈭䈬䈱ㅒ⋧♽䉦䊤䊛䈱ઁ䈮䇮㗅⋧♽䉇㪟㪠㪣㪠㪚䈭䈬䈱䉦䊤䊛䉅↪ᗧ䈚䈩䈇䉁䈜䇯
䉰䊮䊒䊦䈮ᔕ䈛䈢䉦䊤䊛䉕ㆬᛯ䈪䈐䉁䈜䇯䇭㶎ಽข䉦䊤䊛䈱䊤䉟䊮䉝䉾䊒䈫⹦⚦䈲䉟䊅䊷䊃䉲䊦✚ว䉦䉺䊨䉫䉕ෳᾖ䈚䈩䈒䈣䈘䈇䇯
ౝᓘߩ⇣ߥࠆࠞ࡜ࡓߩᕈ⢻Ყセ
Conditions
System
Column
Eluent
Flow Rate
Col.Temp
Col.Pres.
Detection
Sample
ౝᓘOOࠍߣߒߚᤨߩ
ࠨࡦࡊ࡞⽶⩄㊂ߩᲧ₸
୚
4.6 m m I.D .
A s y = 1.03 , N = 2 2,00 0
୚
6.0 m m I.D .
A s y = 1.04 , N = 2 2,00 0
୚
7.6 m m I.D .
A s y = 1.04 , N = 2 0,00 0
୚
1 0 m m I.D .
A s y = 1.04 , N = 2 0,00 0
୚
NEW A s y = 1.04 , N = 2 0,00 0
୚
2 0 m m I.D .
A s y = 1.02 , N = 2 0,00 0
୚
3 0 m m I.D .
A s y = 1.07 , N = 2 0,00 0
୚
5 0 m m I.D .
A s y = 1.08 , N = 1 8,00 0
: PLC 761 system
: Inertsil ODS- 3 (5 μ m, 㐳䈘 250 mm )
ౝᓘ䈲ฦ䉪䊨䊙䊃䉫䊤䊛䈮⸥タ
: A) CH3CN
B) H2 O
A/B = 65/35, v/v
: ✢ㅦᐲ 1 mm/s 䈮ว䉒䈞䈢ᵹ㊂
: 40 ͠
: Approx. 5.0 MPa
: UV 254 nm
: 1. Acetophenone
2. Benzene
3. Toluene
4. Naphthalene
1 4 m m I.D .
+PGTVUKNࠪ࡝࡯࠭ߩಽขࠞ࡜ࡓߪ‫ޔ‬ᄢญᓘࠞ࡜ࡓߢ߽
ࡇ࡯ࠢᒻ⁁߿ℂ⺰Ბᢙ߇⛽ᜬߐࠇࠆߚ߼‫ޔ‬ಽᨆࠞ࡜ࡓ
߆ࠄߩࠬࠤ࡯࡞ࠕ࠶ࡊ߇ࠬࡓ࡯࠭ߦⴕ߃߹ߔ‫ޓޕ‬
0
2
4
6
8
Tim e (m in .)
10
12
14
ౝᓘߩ㆑޿ߦࠃࠆࠢࡠࡑ࠻ࠣ࡜ࡓߩᲧセ
Conditions
System
Column
Eluent
Flow Rate
Col.Temp.
Detection
Sample
: GL- 7400 HPLC system
: Inertsil ODS- 3 (5 μ m, 㐳䈘 250 mm )
ౝᓘ䈲ฦ䉪䊨䊙䊃䉫䊤䊛䈮⸥タ
: A) CH 3 CN
B) 0.1 % TFA
A/B = 40/60, v/v
: ฦ䉪䊨䊙䊃䉫䊤䊛䈮⸥タ
: 40 ͠
: UV 270 nm
: Ꮢ⽼↞⨲᛽಴ᶧ (2.0 mg/ mL)
㩿㪌㪇㩷㩼䊜䉺䊉䊷䊦᛽಴䋩
1. Glycyrrhizic acid
㧝
㧝
0
2
4
6
8
10
Time (min)
ࠞ࡜ࡓౝᓘ 㪈㪋㩷㫄㫄㩷
⽶⩄㊂OI
ࠞ࡜ࡓౝᓘ 㪈㪇㩷㫄㫄㩷
⽶⩄㊂OI
ᵹ㊂
㩷㩷㩷㪐㩷㫄㪣
㪆㫄㫀㫅
ᵈ౉㊂ 㪈㪅㪌㩷㫄㪣
ᵹ㊂
ᵈ౉㊂
12
14
0
16
2
4
6
8
10
Time (min)
12
14
㪋㪅㪌㩷 㫄㪣 㪆㫄㫀㫅
㪎㪌㪇㩷 㱘 㪣
16
⋡⊛ᚑಽߩࡇ࡯ࠢߩㄭߊߦ
ᄳ㔀ᚑಽߩࡇ࡯ࠢ߇޽ࠆ႐ว‫ޔ‬
⽶⩄㊂ࠍჇടߐߖࠆߣࡇ࡯ࠢ߇
㊀ߥࠅ‫⵾♖ޔ‬ല₸߇ᖡߊߥࠅ߹ߔ‫ޕ‬
⽶⩄㊂ࠍ୚ߦߒߡ߽‫ޔ‬ౝᓘOOߣ
ห᭽ߩࠢࡠࡑ࠻ࠣ࡜ࡓ߇ᓧࠄࠇ߹ߔ‫ޕ‬
ᄢ㊂ߦಽขߔࠆ႐วߦ᦭ലߢߔ‫ޕ‬
ଔᩰ⴫䋨☸ሶᓘ㩷㪌㩷㱘㫄㩷䇮ౝᓘ㩷㪈㪋㩷㫄㫄㩷䇮㐳䈘㩷㪉㪌㪇㩷㫄㫄㩷㪀
లႯ೷ฬ
㪠㫅㪼㫉㫋㫊㫀㫃㩷㪦㪛㪪㪄㪋
㪠㫅㪼㫉㫋㫊㫀㫃㩷㪚㪏㪄㪋
㪠㫅㪼㫉㫋㫊㫀㫃㩷㪦㪛㪪㪄㪊
㪠㫅㪼㫉㫋㫊㫀㫃㩷㪦㪛㪪㪄㪪㪧
㪠㫅㪼㫉㫋㫊㫀㫃㩷㪦㪛㪪㪄㪜㪧
㪠㫅㪼㫉㫋㫊㫀㫃㩷㪦㪛㪪㪄㪧
㪠㫅㪼㫉㫋㫊㫀㫃㩷㪚㪏㪄㪊
㪠㫅㪼㫉㫋㫊㫀㫃㩷㪧㪿㪄㪊
㪠㫅㪼㫉㫋㫊㫀㫃㩷㪚㪥㪄㪊
㪚㪸㫋㪅㪥㫆㪅
㪌㪇㪉㪇㪄㪎㪐㪇㪇㪋
㪌㪇㪉㪇㪄㪎㪐㪇㪇㪐
㪌㪇㪉㪇㪄㪎㪐㪇㪈㪋
㪌㪇㪉㪇㪄㪎㪐㪇㪈㪐
㪌㪇㪉㪇㪄㪎㪐㪇㪉㪋
㪌㪇㪉㪇㪄㪎㪐㪇㪉㪐
㪌㪇㪉㪇㪄㪎㪐㪇㪊㪋
㪌㪇㪉㪇㪄㪎㪐㪇㪊㪐
㪌㪇㪉㪇㪄㪎㪐㪇㪋㪋
ଔᩰ
㪉㪉㪇㪃㪇㪇㪇
㪉㪉㪇㪃㪇㪇㪇
㪈㪐㪏㪃㪇㪇㪇
㪈㪐㪏㪃㪇㪇㪇
㪈㪐㪏㪃㪇㪇㪇
㪈㪐㪏㪃㪇㪇㪇
㪈㪐㪏㪃㪇㪇㪇
㪈㪐㪏㪃㪇㪇㪇
㪈㪐㪏㪃㪇㪇㪇
లႯ೷ฬ
㪠㫅㪼㫉㫋㫊㫀㫃㩷㪥㪟㪉
㪠㫅㪼㫉㫋㫊㫀㫃㩷㪛㫀㫆㫃
㪠㫅㪼㫉㫋㫊㫀㫃㩷㪪㪠㪣㪄㪈㪇㪇㪘
㪠㫅㪼㫉㫋㫊㫀㫃㩷㪮㪧㪊㪇㪇㩷㪚㪈㪏
㪠㫅㪼㫉㫋㫊㫀㫃㩷㪮㪧㪊㪇㪇㩷㪚㪏
㪠㫅㪼㫉㫋㫊㫀㫃㩷㪮㪧㪊㪇㪇㩷㪚㪋
㪠㫅㪼㫉㫋㫊㫀㫃㩷㪮㪧㪊㪇㪇㩷㪛㫀㫆㫃
㪠㫅㪼㫉㫋㫊㫀㫃㩷㪮㪧㪊㪇㪇㩷㪪㪠㪣
㪚㪸㫋㪅㪥㫆㪅
㪌㪇㪉㪇㪄㪎㪐㪇㪋㪐
㪌㪇㪉㪇㪄㪎㪐㪇㪌㪋
㪌㪇㪉㪇㪄㪎㪐㪇㪌㪐
㪌㪇㪉㪇㪄㪎㪐㪇㪎㪋
㪌㪇㪉㪇㪄㪎㪐㪇㪎㪐
㪌㪇㪉㪇㪄㪎㪐㪇㪏㪋
㪌㪇㪉㪇㪄㪎㪐㪇㪏㪐
㪌㪇㪉㪇㪄㪎㪐㪇㪐㪋
ଔᩰ
㪈㪐㪏㪃㪇㪇㪇
㪈㪐㪏㪃㪇㪇㪇
㪈㪐㪏㪃㪇㪇㪇
㪉㪌㪇㪃㪇㪇㪇
㪉㪌㪇㪃㪇㪇㪇
㪉㪌㪇㪃㪇㪇㪇
㪉㪌㪇㪃㪇㪇㪇
㪉㪌㪇㪃㪇㪇㪇
̪਄⸥એᄖߩࠨࠗ࠭ߦ㑐ߒߡߪ‫ޔ‬೎ㅜ߅໧޿วࠊߖߊߛߐ޿‫ޕ‬
䃂䈖䈱䉦䉺䊨䉫䈱⵾ຠ䈲ᡷ⦟䈱䈢䉄ᄖⷰ䇮઀᭽䈱৻ㇱ䉁䈢䈲ଔᩰ䉕ᄌᦝ䈜䉎䈖䈫䈏䈅䉍䉁䈜䇯
䃂ળ␠ฬ䇮⵾ຠฬ╬䈲৻⥸䈮ฦ␠䈱໡ᮡ䈍䉋䈶⊓㍳໡ᮡ䈪䈜䇯
4
䃂ᧄᢥਛ䈮䈲㪫㪤䈍䉋䈶㩷㩷㩷㩷䊙䊷䉪䈲᣿⸥䈚䈩䈍䉍䉁䈞䉖䇯
䃂ᧄᢥਛ䈮ឝタ䈚䈩䈇䉎ଔᩰ䈮䈲ᶖ⾌⒢╬䈲฽䉁䉏䈩䈇䉁䈞䉖䇯
ㇱ
ᐫ
ᐫ
ᚲ
ᚲ
ᚲ
ᚲ
ᚲ
ᚲ
ᚲ
㪫㪜㪣㪅㪇㪊䋨㪌㪊㪉㪊䋩㪍㪍㪈㪈
㪫㪜㪣㪅㪇㪍䋨㪍㪊㪌㪎䋩㪌㪇㪍㪇
㪫㪜㪣㪅㪇㪋㪌䋨㪐㪏㪌䋩㪎㪐㪇㪇
㪫㪜㪣㪅㪇㪉㪋䋨㪌㪊㪊䋩㪉㪉㪋㪋
㪫㪜㪣㪅㪇㪉㪐䋨㪏㪌㪏䋩㪊㪎㪇㪇
㪫㪜㪣㪅㪇㪋㪊䋨㪉㪋㪏䋩㪉㪋㪋㪈
㪫㪜㪣㪅㪇㪋㪏䋨㪍㪍㪎䋩㪈㪍㪈㪈
㪫㪜㪣㪅㪇㪌㪉䋨㪐㪊㪈䋩㪈㪎㪍㪈
㪫㪜㪣㪅㪇㪏㪉䋨㪉㪊㪊䋩㪈㪈㪇㪈
㪫㪜㪣㪅㪇㪐㪉䋨㪉㪐㪈䋩㪌㪉㪇㪇
㪝㪘㪯㪅㪇㪊䋨㪌㪊㪉㪊䋩㪍㪍㪉㪉
㪝㪘㪯㪅㪇㪍䋨㪍㪊㪌㪎䋩㪋㪌㪏㪇
㪝㪘㪯㪅㪇㪋㪌䋨㪐㪏㪌䋩㪎㪐㪇㪈
㪝㪘㪯㪅㪇㪉㪋䋨㪌㪊㪍䋩㪈㪌㪈㪏
㪝㪘㪯㪅㪇㪉㪐䋨㪏㪌㪏䋩㪊㪎㪏㪇
㪝㪘㪯㪅㪇㪋㪊䋨㪉㪋㪏䋩㪉㪋㪏㪌
㪝㪘㪯㪅㪇㪋㪏䋨㪍㪍㪎䋩㪈㪍㪌㪍
㪝㪘㪯㪅㪇㪌㪉䋨㪐㪊㪈䋩㪈㪏㪈㪋
㪝㪘㪯㪅㪇㪏㪉䋨㪉㪊㪊䋩㪈㪈㪈㪇
㪝㪘㪯㪅㪇㪐㪉䋨㪉㪐㪈䋩㪉㪌㪌㪉
✚ ว ᛛ ⴚ ᧄ ㇱ
㪫㪜㪣㪅㪇㪋䋨㪉㪐㪊㪋䋩㪉㪈㪉㪈
㪫㪜㪣㪅㪇㪋䋨㪉㪐㪊㪋䋩㪈㪈㪇㪇
㪫㪜㪣㪅㪇㪉㪋䋨㪌㪊㪊䋩㪉㪉㪋㪋
㪝㪘㪯㪅㪇㪋䋨㪉㪐㪊㪋䋩㪉㪈㪉㪏
㪝㪘㪯㪅㪇㪋䋨㪉㪐㪊㪋䋩㪊㪊㪍㪈
㪝㪘㪯㪅㪇㪉㪋䋨㪌㪊㪋䋩㪉㪈㪊㪐
᧲ ੩ ༡ ᬺ
ᄢ
㒋
ᡰ
ᮮ
ᵿ
ᡰ
᧲ ർ ༡ ᬺ
╳ ᵄ ༡ ᬺ
ජ ⪲ ༡ ᬺ
ർ 㑐 ᧲ ༡ ᬺ
ฬ ฎ ደ ༡ ᬺ
ᐢ ፉ ༡ ᬺ
਻ Ꮊ ༡ ᬺ
䉦䉴䉺䊙䊷䉰䊘䊷䊃䉶䊮䉺䊷
⑔
ፉ
Ꮏ
႐
ᧄ䇭␠䇭䇾㪈㪍㪊㪄㪈㪈㪊㪇㩷㩷᧲੩ㇺᣂኋ඙⷏ᣂኋ㪍ৼ⋡㪉㪉⇟㪈ภ㩷㩷ᣂኋ䉴䉪䉣䉝䉺䊪䊷㪊㪇㪝
䇭䇭䇭䇭㪫㪜㪣㪅㪇㪊䋨㪌㪊㪉㪊䋩㪍㪍㪈㪈䇭㪝㪘㪯㪅㪇㪊䋨㪌㪊㪉㪊䋩㪍㪍㪉㪉
䇭䇭䇭䇭㪿㫋㫋㫇㪑㪆㪆㫎㫎㫎㪅㪾㫃㫊㪅㪺㫆㪅㫁㫇㩷 㪼㪄㫄㪸㫀㫃㪑㫀㫅㪽㫆㪗㪾㫃㫊㪅㪺㫆㪅㫁㫇
቟ో䈮㑐䈜䉎䈗ᵈᗧ
2&(
䈗૶↪೨䈮䇸ขᛒ⺑᣿ᦠ䇹䉕䉋䈒䈍⺒䉂䈱਄䇮ᱜ䈚䈒૶↪䈚䈩䈒䈣䈘䈇䇯