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START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 1 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 2 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd The products described in this manual are subject to continuous development and improvement and it is therefore acknowledged that this manual may contain errors or omissions. EiUK Eurotron Instruments (UK) ltd encourage customer feedback and welcome any comments or suggestions relating to the product or documentation. These should be forwarded to the Customer Feedback Department at the address given below. Eurotron Instruments (UK) ltd Unit 13 Riley Close, Royal Oak Industrial Estate, Daventry, NN11 8QT, England Tel: +44 (0)1327 871044 Fax: +44 (0)1327 301255 Email: [email protected] www.eurotronuk.com This manual is intended as a guide to use this product. Eurotron Instruments (UK) ltd shall not be liable for any loss or damage whatsoever arising from the wrong comment / interpretation of information’s from this manual or any misuse come out of this manual. Attention! Inspect shipments in the presence of deliverer. If necessary remove packaging material and have damages to packaging and goods confirmed on the packing slip. Any such notice must be received by EiUK Eurotron Instruments (UK) ltd within 3 days upon receipt of package. Otherwise they could not be admitted! Save the original box and the packing material to protect in case you have to ship or transport it. 3 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 1 Content 1 Content ............................................................................................................................................................. 4 2 Measuring principle........................................................................................................................................... 7 3 4 2.1 Electrochemical measuring principle ........................................................................................................ 7 2.2 NDIR- measurement ................................................................................................................................. 8 2.3 Gas flow chart RASI 900 .......................................................................................................................... 9 2.4 Gas flow chart RASI 901 ........................................................................................................................ 10 Device views.................................................................................................................................................... 11 3.1 Right side view RASI 900 ...................................................................................................................... 11 3.2 Left side view RASI 900.......................................................................................................................... 11 3.3 Right side view RASI 901 ...................................................................................................................... 12 3.4 Left side view RASI 901.......................................................................................................................... 12 3.5 Condensate separator RASI 900............................................................................................................. 13 Prepare for measurement................................................................................................................................ 14 4.1 Printer .................................................................................................................................................... 15 4.1.1 Printing procedure ............................................................................................................................. 15 4.1.2 Handling the printer........................................................................................................................... 15 4.1.2.1 How to open the cover assembly.............................................................................................. 15 4.1.2.2 How to load paper rolls ............................................................................................................ 15 4.1.2.3 How to close the cover correctly and cut the paper.................................................................. 15 5 6 7 Base of calculation .......................................................................................................................................... 16 5.1 Analysis and calculation......................................................................................................................... 16 5.2 Combustion calculations ........................................................................................................................ 16 Technical specifications................................................................................................................................... 17 6.1 RASI 900 ................................................................................................................................................ 17 6.2 RASI 901 ................................................................................................................................................ 18 Probes RASI 900.............................................................................................................................................. 21 7.1 Probe unheated...................................................................................................................................... 21 7.2 Probe unheated with sintered metal filter .............................................................................................. 22 7.2.1 Change of the sintered metal filter .................................................................................................... 23 7.2.2 Handling of the quick hook-up connector.......................................................................................... 23 7.3 Probe with heated glass wool filter........................................................................................................ 24 7.3.1 Replace glass wool filter elements of industrial gas sampling probe................................................. 25 7.3.2 Probe with heated sintered metal tube filled with glass wool material (option)................................ 25 8 Probes RASI 901.............................................................................................................................................. 26 8.1 Probe unheated...................................................................................................................................... 26 8.1.1 Handling of the quick hook-up connector.......................................................................................... 27 8.2 Probe unheated with sintered metal filter .............................................................................................. 28 8.2.1 Change of the sintered metal filter .................................................................................................... 29 8.3 Probe with heated glass wool filter........................................................................................................ 30 8.3.1 Replace glass wool filter elements of industrial gas sampling probe................................................. 31 8.3.2 Probe with heated sintered metal tube filled with glass wool material (option)................................ 32 4 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 8.4 Probe with heated glass wool filter and heated sample line .................................................................. 33 8.4.1 Connection of the heated hose.......................................................................................................... 34 8.4.2 Handling of the quick hook-up connector.......................................................................................... 34 9 Default ............................................................................................................................................................ 35 9.1 10 11 Error diagnosis regarding the analyser................................................................................................... 35 Maintenance ................................................................................................................................................... 36 10.1 Insideview .............................................................................................................................................. 36 10.2 Sample gas filter (RASI 900)................................................................................................................... 37 10.3 Sample gas filter / PTFE (RASI 901) ........................................................................................................ 37 10.4 Servicing fine filter # 56066 ................................................................................................................... 38 10.5 NOx protection filter (PURAFIL).............................................................................................................. 40 10.6 Servicing Acrodisc # 51513 (option)....................................................................................................... 40 10.7 Change the mains fuses ......................................................................................................................... 41 10.8 Change the lithium battery for sensor BIAS voltage supply.................................................................... 42 10.9 Servicing gas pump # 55513 .................................................................................................................. 43 10.10 Servicing CO purging pump # 54151 ................................................................................................. 45 10.11 Servicing CO purge solenoid valve # 59687....................................................................................... 46 10.12 Replace O2 sensor # 58048A............................................................................................................. 47 10.13 Dismount the gas cooler (RASI 901) .................................................................................................. 48 Adjustment...................................................................................................................................................... 53 11.1 Adjust temperatures............................................................................................................................... 53 11.1.1 Adjust offset of the thermocouple T-air amplifier.......................................................................... 54 11.1.2 Adjust offset of the thermo couple T-gas amplifier ....................................................................... 54 11.1.3 Adjust span of the thermo couple T air amplifier .......................................................................... 54 11.1.4 Adjust span of the thermo couple T gas amplifier......................................................................... 54 11.1.5 Adjust span of the temperature reference..................................................................................... 55 11.1.6 Adjust span of the temperature reference T-air amplifier.............................................................. 55 11.1.6.1 Adjust span of the temperature reference T-gas amplifier........................................................ 55 11.2 Adjust Pressure....................................................................................................................................... 56 11.2.1 Adjustment of the lower range ..................................................................................................... 56 11.2.2 Adjustment of the upper range ..................................................................................................... 56 11.3 AUX channel adjustment........................................................................................................................ 57 11.3.1 Adjustment thermocouple AUX amplifier...................................................................................... 58 11.3.2 Adjustment 0-10V AUX ................................................................................................................. 58 11.3.3 Adjustment 4-20mA ...................................................................................................................... 58 11.4 Analog output (4 - 20mA) ...................................................................................................................... 59 12 Service maintenance plan................................................................................................................................ 60 13 Self diagnosis .................................................................................................................................................. 60 13.1 Sensors: ( to fresh air ) ........................................................................................................................... 60 13.2 Battery voltage....................................................................................................................................... 60 13.3 Temperatures ......................................................................................................................................... 61 13.4 Draft....................................................................................................................................................... 61 13.5 Bias-voltage ........................................................................................................................................... 61 5 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 14 13.6 KTY-chart ............................................................................................................................................... 61 13.7 PT2000-chart.......................................................................................................................................... 61 Appendix ......................................................................................................................................................... 62 14.1 Manual for firmware update of H8-Industrial analyzers......................................................................... 62 14.1.1 System requirements..................................................................................................................... 62 14.1.2 Important hints and warnings ....................................................................................................... 62 14.1.3 Update procedure ......................................................................................................................... 62 14.1.4 Possible causes and solutions in case of update failure: ............................................................... 62 14.2 Electrical connections............................................................................................................................. 63 14.2.1 Analog output ............................................................................................................................... 63 14.2.2 RS 232 connector .......................................................................................................................... 63 14.2.3 RS 485 connector .......................................................................................................................... 63 14.2.4 RS 485 converter connection to PC ............................................................................................... 64 14.2.5 RS 232 connection to PC ............................................................................................................... 66 14.3 Transmission protocol ............................................................................................................................ 67 14.3.1 Online data transmission protocol ................................................................................................ 67 14.3.2 data storage transmission protocol ............................................................................................... 68 14.4 Display messages ................................................................................................................................... 69 14.5 Lists of countries and fuel types ............................................................................................................. 72 14.5.1 General information ...................................................................................................................... 72 14.5.1.1 CO2, Lambda, losses, efficiency................................................................................................ 72 14.5.1.2 Dew point ................................................................................................................................. 72 14.5.1.3 CO- conversion of CO [ppm] ..................................................................................................... 72 14.5.1.4 NO-conversion of NO [ppm] ..................................................................................................... 73 14.5.1.5 NO2-conversion of NO2 [ppm] ................................................................................................. 73 14.5.1.6 NOx-conversion of NO [ppm] (possible also of NO2 [ppm]) ..................................................... 73 14.5.2 Fuel type list Great Britain............................................................................................................. 74 6 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 2 Measuring principle The measurement principle of toxic gases is based on the electrochemical principle or optionally on infrared bench (NDIR). Temperatures are measured by means of thermocouples Type K (NiCrNi) , optionally type S ( PtRhPt) for very high temperature probe and Platinum RTD PT 2000. 2.1 Electrochemical measuring measuring principle The oxygen content of the sample gas will be measured with a 2 electrodes electrochemical sensor. Toxic gases like carbon monoxide CO, nitrogen oxide NO, nitrogen dioxide NO2, sulfur dioxide SO2 ,hydrogen sulphide H2S will be measured with 3-electrodes sensors. The electrochemical sensors are based on the gas diffusion technology. The advantages of this technology are: The permanently generated signal is direct proportionally and linear to the volume concentration (% or ppm) of the analysis gas components. The 3 electrodes are: S (sensing electrode), C (counter electrode) and R (reference electrode). Pos. 1 2 3 4 5 6 7 8 9 Messgas Staubfilter S-Elektrode R-Elektrode C-Elektrode Anschlusspin Elektrolytspeicher Elektrolyt Kapillarmembrane Sample gas Particle filter Sensing electrode Reference electrode Counter electrode Connecting pin Electrolyte reservoir Bilk electrolyte Capillary diffusion barrier The gases reaches the sensing electrode reacts on the electrode surface either through oxidation ( for example CO, H2S, SO2, NO, H2 ) or reduction (like CO, H2S, SO2, NO, H2 ) Example: CO sensor: CO reacts at the sensing electrode as follows: CO + H2O - > CO2 + 2H+ + 2eotherwise: at the counter electrode oxygen from air will be re-oxidize to water: ½ O2 + 2H+ + 2e 2 e - - > H 2O The generated current (µA-range) will be measured and analysed by the microprocessor. 7 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 2.2 NDIRNDIR- measurement By means of the non-disperse infrared bench of the RASI 901, it is possible to measure carbon monoxide (CO), carbon dioxide (CO2) and hydro-carbons (HC). Optional it is possible to measure sulphur dioxide SO2 in higher ranges as it is possible with the electrochemical SO2 sensor. Principle of the IRIR- bench A regulated infrared source (IR) provides a photon stream in the range of 2 to 8 microns (µm). The infrared light is directed through the sample cell to the optical detector. The source is electronically modulated with 2Hz ( no chopper wheels, no moving parts). Infrared transparent calcium fluoride lens are provided at each end of the gas sample cell. The pyro-electric detector is temperature regulated. Additionally a measurement compensation for the sample gas temperature and pressure variations is provided. The residual infrared energy, not absorbed by the sample gas, is guided to the optical detector. It passes four optical narrow band pass filter that are each aligned on the infrared absorption spectrum of the target gases (one filter is the reference filter; it is used for ageing and soiling compensation). Infrared light passed through the filter is collected by four pyro-electric detectors, which share the same housing. They produce a voltage that is proportional to light intensity. The detector block temperature measurement and regulation facilitates compensation for IR filter and IR detector temperature variances. The detector out-put is preamplified and sent via a multiplexer to an analog or to a digital converter (ADC) and to the u-controller. 8 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 2.3 Gas flow chart RASI 900 9 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 2.4 Gas flow chart RASI 901 90 1 10 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 3 3.1 Device views Right side view RASI 900 Position 1 2 3 3 5 6 3.2 Thermoprinter RS 232 interface (8x) Analog outputs 4 – 20 mA (option) Mains fuse ( 2x 3,16A slow) Universal power supply 90 – 240 Vac SD Card (option) Left side view RASI 900 Position 1 2 3 4 5 6 7 8 11 Connector combustion air temperature Condensate outlet Sample gas inlet Connector heated probe Differential pressure port P Differential pressure port P + Condensate seperator Gasfilter START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 3.3 Right side view RASI 901 901 Position 1 2 3 4 5 6 7 8 9 3.4 Thermoprinter RS 232 interface (8x) Analog outputs 4 – 20 mA (option) Mains fuse ( 2x 3,16A slow) Universal power supply 90 – 240 Vac SD Card (option) External keyboard External 12 Vdc power supply RS 485 Left side view RASI 901 90 1 Position 1 2 3 4 5 6 7 8 9 10 12 Connector combustion air temperature Condensate outlet Sample gas inlet Connector heated probe Differential pressure port P Differential pressure port P + not connectred Ventilation gas cooler AUX connector Filter (PTFE) START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 3.5 Condensate separator RASI 900 Pos. 1 2 3 4 5 6 7 8 9 10 11 12 13 # 56439 11165 51517 62279 62269 56124 51516 59169 62278 51317 51516 52359 cover filter O-ring O-ring fitting center part 2 x O-ring high-grade steel pipe high-grade steel pipe condensate vessel O-ring plug START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 4 Prepare for measurement It is necessary to check before even measurement the condensate separator. The separator must be clean (without (without condensate) and the filter has to be white coloured! coloured! If the filter is contaminated, it changes the colour from white to grey/brown and is has be washed up to 5 times (e.g. ultrasonic bath) or replaced! (Start-up with other available probes see § 7) • Take out analyser from the transport case • Mount gas sample probe and connect it to the analyser. Connect RASI to mains power supply It can be power supplied by: 1. 90-240 Vac mains power supply, 100 W, with mains power cable 2. Internal battery 12V, 1800mAh and switch on by pressing • Zero calibration is carried out for at least 2 minutes, max. 4 minutes. During this period of time, the measuring cells of the analyser are purged with ambient air. Flue gas measurement cannot be started. All other menu items can be selected. • If the option NDIR bench is installed, you have to consider the warm-up time of the bench • After the zero calibration the RASI is ready to carry out flue gas measurements Long term nonnon- operating and storage: 1. charge battery every 4 weeks 2. store in a dry place 14 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 4.1 4.1.1 Printer Printing procedure The printing procedure can be started in the menus: Measurement, View Last Values, Save Measurement, View Stored Data, Service or Adjustment. Press printer key in the according menu 4.1.2 4.1.2.1 Handling Handling the printer How to open the cover assembly Lift the lever, acting as indicated by the arrow, until the cover is released from its locking position. To avoid damages to the lever, do not use excessive force 4.1.2.2 How to load paper rolls 4.1.2.3 How to close close the cover correctly and cut the paper Press on both sides of the cover group (simultaneously) (A). Alternatively: Press on the middlle of cover group (near the paper exit) (B). Do not close the cover by pressing only one side! How to cut the paper: Pull the paper towards the tear bar from one side to the other. 15 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 5 Base of calculation 5.1 Analysis and calculation Continuously measured items Unit Stan Standard O2 [%] X CO [ppm] X NO [ppm] option NO2 [ppm] option SO2 [ppm] option H 2S [ppm] option Air temperature (thermocouple) [°C] X Flue gas temperature (thermocouple) [°C] X Draft [hPa] and others option Differential pressure [hPa] and others option Calculations: Continuous transformation [ ppm ] X [ ppm ] in reference to O2 reference value X 3 X 3 X [ mg/m ] [ mg/m ] in reference to O2 reference value Other calculated values Unit CO2 [%] Efficiency (ETA) * [%] Losses * [%] Excess air - Dew point [°C] PI = Poison index (ratio from CO to CO2) [%] Losses and efficiency are calculated by means of net calorific value. These values are than referenced for the gross calorific value for condensing boilers only. (efficiency > 100) Formula for calculation poison index : PI [%] = 100 x CO [ppm] / CO2 [ppm] 5.2 Combustion calculations The calculation of efficiency and the exhaust losses is carried out according to the formula of Siegert: (see chapter 14.5.1) 14.5.1 16 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 6 6.1 Technical specifications RASI 900 electrochemical cell O2 Range Accuracy CO (H2 comp.) Range Accuracy NO [Option # 59699] Range Accuracy NO2 [Option # 59731] Range Accuracy SO2 [Option # 59732] Range Accuracy H2S [Option # 59730] Range Accuracy with NDIR MultiMulti -gas bench CO Range Accuracy CO2 Range Accuracy CXHY equiv CH4 Range Accuracy with NDIR MultiMulti -gas bench CO Range Accuracy CO2 Range Accuracy CXHY equiv C3H8 Range Accuracy temperaturee TA Stack gas temperatur Range Range Range Accuracy 0 - 21,0 Vol-% ± 0,2 Vol-% abs. 0 - 2.000 ppm, overload up to 4.000 ppm ± 10 ppm or 5 % reading 4.000 ppm 10 % reading > 4.000 ppm 0 - 1.000 ppm, overload up to 5.000 ppm ± 5 ppm or 5 % reading 1.000 ppm 10 % reading > 1.000 ppm 0 - 200 ppm, overload up to 1.000 ppm ± 5 ppm or 5 % reading 200 ppm 10 % reading > 200 ppm 0 - 2.000 ppm, overload up to 5.000 ppm ± 10 ppm or 5 % reading 2000 ppm 10 % reading > 2000 ppm 0 - 50 ppm, overload up to 500 ppm ± 5 ppm or 5 % reading 50 ppm 10 % reading > 50 ppm # 58118, 65 mm, CO, CO2, CH4 min. 0 - 3 % up to max.0 - 10 % ± 0,03 % or 5 % reading min. 0 - 3 % up to max. 0 - 30 % ± 0,5 % or 5 % reading min. 0 - 1 % up to max. 0 - 3 % equiv. CH4 ± 0,01 % or 5 % reading # 58986, 65 mm, CO, CO2, C3H8 min. 0 - 3 % up to max.0 - 10 % ± 0,03 % or 5 % reading min. 0 - 3 % up to max. 0 - 30 % ± 0,5 % or 5 % reading min. 0 - 2.000 ppm up to max. 0 - 5.000 ppm equiv. C3H8 ± 30 ppm or 5 % reading 0 - 650 °C by means of stainless steel sampling tube 0 - 1.100 °C by means of Inconel steel sampling tube 0 - 1.750 °C by means of ceramic sampling tube ± 2 °C 200 °C 17 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd Combustion air temperature T L Range Accuracy Draft Range Accuracy Differential pressure (option) Range Accuracy Flow Range Accuraccy 0 - 100 °C ± 1 °C ± 100 hPa ± 0,02 hPa or 1% reading ± 100 hPa ± 0,02 hPa or 1% reading 1 m/sec up to 100 m/sec ± 1 m/sec or 1 % reading Suction capacity capa city of gas pump 150 hPa Calculated values (depends on fuel type) CO2 Range Accuracy Dewpoint Losses qA Efficiency ή 0 - CO2 max ± 0,3 Vol-% abs. °C 0 - 99,9 % 0 - 120 % Measured values as mg/Nm3, O2 referenced, NOx as mg/Nm3NO2, mg/sec General specifications Operation temperature Storage temperture Power supply Protection class Weight Dimensions + 5 - + 45 °C, max. 95 % humidity, not condensing - 20 - + 50 °C Universal grid power 100 - 250 Vac, 47 - 63 Hz 12 V / 3,6 Ah internal battery, operation 8 hour IP 21 approx. 7kg (without case and accessories) 530 x 490 x 310 mm Technical changes without notice! 6.2 Date of issue 20110530 RASI 901 90 1 Measured Measu red values electrochemical cell O2 Range Accuracy CO (H2 comp.) Range Accuracy NO [Option # 59699] Range Accuracy NO2 [Option # 59731] Range Accuracy 0 - 21,0 Vol-% ± 0,2 Vol-% abs. 0 - 2.000 ppm, overload up to 4.000 ppm ± 10 ppm or 5 % reading 4.000 ppm 10 % reading > 4.000 ppm 0 - 1.000 ppm, overload up to 5.000 ppm ± 5 ppm or 5 % reading 1.000 ppm 10 % reading > 1.000 ppm 0 - 200 ppm, overload up to 1.000 ppm ± 5 ppm or 5 % reading 200 ppm 18 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 10 % reading > 200 ppm SO2 [Option # 59732] Range Accuracy H2S [Option # 59730] Range Accuracy H2 [Option # 60270] Range Accuracy CO very high [Option # 59939] Range Accuracy with NDIR MultiMulti -gas bench CO Range Accuracy CO2 Range Accuracy CXHY equiv CH4 Range Accuracy with NDIR MultiMulti -gas bench CO Range Accuracy CO2 Range Accuracy CXHY equiv CH4 Range Accuracy with NDIR MultiMulti -gas bench CO Range Accuracy CO2 Range Accuracy CXHY equiv C3H8 Range Accuracy Stack gas temperature TA Range Range Range Accuracy 0 - 2.000 ppm, overload up to 5.000 ppm ± 10 ppm or 5 % reading 2000 ppm 10 % reading > 2000 ppm 0 - 50 ppm, overload up to 500 ppm ± 5 ppm or 5 % reading 50 ppm 10 % reading > 50 ppm 0 - 1 %, overload up to 2 % ± 0,02 % or 5 % reading 1 % 10 % reading > 1 % 0 - 4,00 %, overload up to 10,00 % ± 0,02 % or 5 % reading 4 % 10 % reading > 4 % # 61447, 103 mm, CO, CO2, CH4 min. 0 - 10.000 ppm up to max.0 - 30.000 ppm ± 40 ppm or 5 % reading min. 0 - 3 % up to max. 0 -20 % ± 0,5 % or 5 % reading min. 0 - 10.000 ppm up to max. 0 - 30.000 ppm equiv. CH4 ± 60 ppm or 5 % reading # 58118, 65 mm, CO, CO2, CH4 min. 0 - 3 % up to max.0 - 10 % ± 0,03 % or 5 % reading min. 0 - 3 % up to max. 0 - 30 % ± 0,5 % or 5 % reading min. 0 - 1 % up to max. 0 - 3 % equiv. CH4 ± 0,01 % or 5 % reading # 58986, 65 mm, CO, CO2, C3H8 min. 0 - 3 % up to max.0 - 10 % ± 0,03 % or 5 % reading min. 0 - 3 % up to max. 0 - 30 % ± 0,5 % or 5 % reading min. 0 - 2.000 ppm up to max. 0 - 5.000 ppm equiv. C3H8 ± 30 ppm or 5 % reading 0 - 650 °C by means of stainless steel sampling tube 0 - 1.100 °C by means of Inconel steel sampling tube 0 - 1.750 °C by means of ceramic sampling tube ± 2 °C 200 °C 1 % reading > 200 °C 19 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd Combustion air temperature T L Range Accuracy Draft Range Accuracy Differential pressure (option) Range Accuracy ± 100 hPa ± 0,02 hPa or 1% reading Suction capacity of gas pump 150 hPa Flow Range Accuraccy 1 m/sec up to 100 m/sec ± 1 m/sec or 1 % reading Calculated values (depends on fuel type) CO2 Range Accuracy Dewpoint Losses qA Efficiency ή 0 - CO2 max ± 0,3 Vol-% abs. °C 0 - 99,9 % 0 - 120 % Measured values as mg/Nm3, O2 referenced, NOx as mg/Nm3NO2, mg/sec 0 - 100 °C ± 1 °C ± 100 hPa ± 0,02 hPa or 1% reading General specifications Operation temperature Storage temperture Power supply Protection class Weight Dimensions + 5 - + 45 °C, max. 95 % humidity, not condensing - 20 - + 50 °C Universal grid power 100 - 250 Vac, 47 - 63 Hz 12 V / 3,6 Ah internal battery, operation 2 hour IP 21 approx. 7kg (without case and accessories) 530 x 490 x 310 mm Technical changes without notice! Date of issue 2010530 20 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 7 Probes RASI 900 7.1 Probe unheated ! Without filter elements, to be used only for clean combustion site, e.g. natural gas! Gas sample probe for low dust site, with exchangeable probe tube, continuous stack draft measurement, gas temperature measurement up to 650°C ( up to 1100°C with Inconel tube) Item Probe handle with Probe handle with Description Temperature range 2,7 m unheated sample line 5,0 m unheated sample line Probe tube Probe tube Probe tube Probe tube Probe tube 300 mm, Ø 10 mm 750 mm, Ø 10 mm 1.000 mm, Ø 10 mm 1.500 mm, Ø 10 mm 2.000 mm, Ø 10 mm Probe tube Probe tube Inconel 1.000 mm, Ø 10 mm Inconel 1.500 mm, Ø 10 mm 21 # 62222 62223 up to 650°C up to 650°C up to 650°C up to 650°C up to 650°C 55671 55672 55673 55674 55464 up to 1.100°C up to 1.100°C 56737 56738 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 7.2 Probe unheated with sintered metal filter Gas sample probe for increased dust site, with exchangeable probe tube, continuous stack draft measurement, gas temperature measurement. Item Probe handle with Probe handle with Probe tube Probe tube Probe tube Description Description Temperature range 2,7 m unheated sample line 5,0 m unheated sample line 750 mm, Ø 10 mm with sintered metal filter # 56748 1.000 mm, Ø 10 mm with sintered metal filter # 56748 1.500 mm, Ø 10 mm with sintered metal filter # 56748 22 # 59774 59778 up to 500°C up to 500°C up to 500°C 60813 60814 60815 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 7.2.1 Change of the sintered metal filter The sintered metal filter should be controlled daily (dependent on the dusty condition in the exhaust gas) around exact results of measurement to attain. If the filter is dirty, it can be cleaned with the help of an ultrasonic bath (unlimited re-use of the cleaned filter) Unscrew dirty filter! Wear protective gloves! Filter element with compressed air (1) the inside the filter blow out or in an ultrasonic bath clean, Do not damage the thermocouple (2) when from/screwing the filter elements in! 7.2.2 Handling of the quick hookhook- up connector Connect quick connector from hose end by pushing it to gas inlet port of analyser. To remove the probe, press the metal plate of the quick connector and pull it out. 23 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 7.3 Probe with heated glass wool filter Industrial gas sample probe for high dust site, with heated, easy replaceable glass wool filter, exchangeable probe tube, (no stack draft measurement integrated) gas temperature measurement up to 650°C (up to 1100°C with Inconel tube). Stack draft measurement possible with option “Stack draft probe with 3 m silicone hose ” Art-No. 59798) Item Probe handle with Probe handle with Probe tube Probe tube Probe tube Probe tube Probe tube Probe tube Probe tube Probe tube Description Temperature range 2,7 m unheated sample line 5,0 m unheated sample line 300 mm, Ø 12 mm 750 mm, Ø 12 mm 1.000 mm, Ø 12 mm 1.500 mm, Ø 12 mm 2.000 mm, Ø 12 mm Art. No. 62224 62225 up to 650°C up to 650°C up to 650°C up to 650°C up to 650°C 11620 11621 11622 11623 11624 Inconel, 1.000 mm, Ø 12 mm up to 1100°C Inconel, 1.500 mm, Ø 12 mm up to 1100°C Inconel, 2.000 mm, Ø 12 mm up to 1100°C 59552 59904 59622 24 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 7.3.1 Replace glass wool filter elements of industrial gas sampling probe probe (only for probes # 62224 and 62225) If the filter element changes from white to grey/brown the glass wool must be replace. Press the filter cartridge 3 mm against the spring, then turn left 45° (bayonet lock) Take out the glass wool by means of a tweezers. Use protection gloves, the exhausted glass wool can be acid-containing! The probe handle can be hot!° Of new glass wool approx. 2 g weight out, insert and into the filter cartridge by means of tweezers. The drillings (1) of the filter cartridge must be on the catch side! If the O-rings (2) # 61066 and / or (3) # 59799 are damaged, then these O-rings has to be changed! The filter cartridge by means of press and 45° clockwise rotation fasten into the probe handle. 7.3.2 Probe with heated sintered metal tube filled with glass wool wool material (option) 1. 2. 3. 4. Probe handle Filter holder Filter O-ring Recommendation: The sintered metal filter should be inspected every day (depending on the dust content of sample gas) to attain precise measuring results. If the filter is dirty it can be cleaned by means of an ultrasonic bath ( unlimited reusing). 25 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 8 Probes RASI 901 901 8.1 Probe unheated ! Use only for clean combustion site, e.g. natural gas! Gas sample probe for low dust site, with exchangeable probe tube, continuous stack draft measurement, gas temperature measurement up to 650°C ( up to 1.100°C with Inconel tube) Item Probe handle with Probe handle with Description Temperature range 2,7 m unheated sample line 5,0 m unheated sample line 59774 59778 Hose coupling Probe tube Probe tube Probe tube Probe tube Probe tube Probe tube Art.Art.- No. 60236 300 mm, Ø 10 mm 750 mm, Ø 10 mm 1.000 mm, Ø 10 mm Inconel 1.000 mm, Ø 10 mm 1.500 mm, Ø 10 mm 2.000 mm, Ø 10 mm 26 up to 650°C up to 650°C up to 650°C up to 1.100°C up to 650°C up to 650°C 55671 55672 55673 56737 55674 55464 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 8.1.1 Handling of the quick hookhook- up connector Connect quick connector from hose end by pushing it to gas inlet port of analyser. To remove the probe, press the metal plate of the quick connector and pull it out. 27 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 8.2 Probe unheated with sintered metal filter Gas sample probe for increased dust site, with exchangeable probe tube, continuous stack draft measurement, gas temperature measurement. Item Probe handle with Probe handle with Probe tube Probe tube Probe tube Description Temperature range 2,7 m unheated sample line 5,0 m unheated sample line 750 mm, Ø 10 mm 1.000 mm, Ø 10 mm 1.500 mm, Ø 10 mm 28 Art. No. 59774 59778 up to 600°C up to 600°C up to 600°C 60813 60814 60815 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 8.2.1 Change of the sintered sintered metal filter The sintered metal filter should be controlled daily (dependent on the dusty condition in the exhaust gas) around exact results of measurement to attain. If the filter is dirty, it can be cleaned with the help of an ultrasonic bath (unlimited re-use of the cleaned filter) Unscrew dirty filter! Wear protective gloves! Filter element with compressed air (1) the inside the filter blow out or in an ultrasonic bath clean, Do not damage the thermocouple (2) when from/screwing the filter elements in! 29 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 8.3 Probe with heated glass wool filter Industrial gas sample probe for high dust site, with heated, easy replaceable glass wool filter, exchangeable probe tube, (no stack draft measurement integrated) gas temperature measurement up to 650°C (up to 1.100°C with Inconel tube and up to 1.700°C with ceramic tube). Stack draft measurement possible with option “Stack draft probe with 3 m silicone hose ” Art-No. 59798) Item Probe handle with Probe handle with Probe tube Probe tube Probe tube Probe tube Probe tube Probe tube Probe tube Probe tube Probe tube with S-type thermocouple Description Temperature range 2,7 m unheated sample line 5,0 m unheated sample line 300 mm, Ø 12 mm up to 650°C 750 mm, Ø 12 mm up to 650°C 1.000 mm, Ø 12 mm up to 650°C Inconel, 1.000 mm, Ø 12 mm up to 1100°C 1.500 mm, Ø 12 mm up to 650°C 2.000 mm, Ø 12 mm up to 650°C Inconel, 2.000 mm, Ø 12 mm up to 1100°C Ceramic, no temperature reading, up to 1.700°C 1.000 mm, Ø 10 mm Ceramic tube , with temperature reading, up to 1.700°C 1.000 mm, Ø 10 mm 30 Art. No. 59782 59784 11620 11621 11622 59552 11623 11624 59622 59948 50863 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd NOTE: Mounting of probe with ceramic sampling tube requires very slow insertion (some 10 cm/min) of this tube into the duct or pipe. This will avoid the thermal shocks on the fragile ceramic tube, which will cause its mechanical dam damage! 8.3.1 Replace glass g lass wool filter elements of industrial gas sampling probe (only for probe handles # 59782, 59784, 59785 and 60119) If the filter element changes from white to grey/brown the glass wool must be replace. Press the filter cartridge 3 mm against the spring, then turn left 45° (bayonet lock) Take out the glass wool by means of a tweezers. Use protection gloves, the exhausted glass wool can be acid-containing! Consider safety data sheet in the appendix! The probe handle can be hot!° Of new glass wool approx. 2 g weight out, insert and into the filter cartridge by means of tweezers. The drillings (1) of the filter cartridge must be on the catch side! If the O-rings (2) # 61066 and / or (3) # 59799 are damaged, then these O-rings has to be changed! The filter cartridge by means of press and 45° clockwise rotation fasten into the probe handle. 31 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 8.3.2 Probe with heated sintered metal tube filled with glass wool material (option) 5. 6. 7. 8. Probe handle Filter holder Filter O-ring Recommendation: The sintered metal filter should be inspected every day (depending on the dust content of sample gas) to attain precise measuring results. If the filter is dirty it can be cleaned by means of an ultrasonic bath ( unlimited reusing ). 32 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 8.4 Probe with heated glass wool filter and heated sample line Industrial gas sample probe for high dust site, with heated, easy replaceable glass wool filter, exchangeable probe tube, gas temperature measurement and temperature regulated sample line. Stack draft measurement possible with option “Stack draft probe with 3 m silicone hose ” Art-No. 59798) Denomination Probe handle with Probe tube Probe tube Probe tube Probe tube Probe tube Probe tube Probe tube Description 3,0 m temperature regulated, heated gas sample line 5,0 m temperature regulated, heated gas sample line 300 mm, Ø 12 mm 750 mm, Ø 12 mm 1.000 mm, Ø 12 mm Inconel 1.000 mm, Ø 12 mm 1.500 mm, Ø 12 mm 2.000 mm, Ø 12 mm Inconel, 2.000 mm, Ø 12 mm 33 TemperatureTemperature- Art.Art.- No. range 59785 60119 up to 650°C up to 650°C up to 650°C up to 1.100°C up to 650°C up to 650°C up to 1.100°C 11620 11621 11622 59552 11623 11624 59622 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 8.4.1 Connection of the heated hose Connect electrical connector from hose end to connector RASI 901. Turn left or right the connector (1) until it snaps in the socket (2). Than screw clockwise back nut (3) 8.4.2 Handling Handling of the quick hookhook- up connector Connect quick connector from hose end to gas inlet port of analyser, by withdrawing the ring (4) and release after plugging (5). 34 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 9 Default 9.1 Error diagnosis regarding the analyser 1. Malfunction Analyser cannot charge the battery in spite of connecting to mains Analyser cannot be switched off by pressing the OFF key. key Inside of the analyser is too cold, analyser not ready for operation. 2. Error Indication No mains indication in the display 3. Cause Cause Fuse (3,15 A T) in the mains socket is burned out none Analyser does not react on any key.. Self test Temperature indication: - - - , - °C Measuring values are not correct No measurement possible Measurement without Self test exact temperature values. Temperature indication: - - - , - °C Wrong measuring values. Measuring range exceeded: Value O2 too high, Values CO and CO2 to low. No measurement possible Display indication “close probe” Wrong temperature measuring values Gas temperature is too hot or alternates 35 4. Solution Replace the fuse(s). Disconnection of the main power plug and press simultaneous the keys F1 and F4. e. g. analyser was stored at a Put the analyser to a warm cold place during winter. room and connect it to the mains and wait for some minutes. Calibrate analyser . Call our after-sales service Analyser cannot be switched Connect the analyser to on or does not react after the mains in order to being switched on. charge the battery. Battery discharge. Thermo element defective, Call our after-sales serbalancing network intervice. rupted or not connected Remove probe from the gas duct and condensate from the probe tube Connection probe – analyser Effect tightness test! not correct. Leakage at By visual control of probe, probe / tube /, pump does tubes, leaking parts could not suck correctly. be found. Probe tube too hot. Let probe tube cool down, Probe is not fixed respecrespectively fix probe tively screwed correctly. tight, measurement is possible now. Probe is not plugged in cor- Check probe plug respecrectly, defective cable in the tively probe line regarding probe line, formation of damages (loose conneccondensate at the probe tip. tion), remove condensate from the probe tip. START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 10 Maintenance 10.1 Insideview Item 1 2 3 4 Description not used not used not used condensate separator with PTFE filter 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 not used not used dust filter not used sample gas pump diff. pressure sensor Acrodisc PTFE filter (option) NDIR bench (option 1-gas or 4-gas) CO purging pump electrochemical sensors manifold CO purge solenoid valve COlow sensor O2 sensor long-life NO sensor (option) NO2 sensor (option) SO2 sensor (option) H2S sensor (option) or CO high (option) NOx protection filter see chapter 3.5 and 10.2 10.2 10.9 10.6 10.10 10.11 10.12 10.5 36 remarks START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 10.2 Sample gas filter (R (RASI 900) 900) Replace the dust and particle filter of the analyser if the colour is changing from white to brown. Solve the filter case and replace the filter cartridge. Do not loose or forget the sealing ring. The filter elements inside the analyser should be changed at the early service in our service agency. 10.3 Sample gas filter / PTFE (RASI (RASI 901 90 1 ) Replace the dust and particle filter of the analyser if the colour is changing from white to brown. Solve the filter case and replace the filter cartridge. Do not loose or forget the sealing ring. OK The filter elements inside the analyser should be changed at the early service in our service agency 37 DIRTY START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 10.4 Servicing fine filter # 56066 If it is necessary to replace the internal filter elements earlier than service interval, open the front panel of the analyser (4 hexagon socket screws): Take the fine filter (1,2 and 3) out of the clamp. Screw up the filter housing and replace the filter pads. The metal screens at the in- and output of the filter housing should be cleaned with compressed air. After cleaning the metal screens and replacing the filter tabs, build in the filter and observe the marked flow direction. Remove the hoses, NOTE: Consider installation direction of the filter (marking)! 38 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd Filter housing screw on and filter tablet take out Take out the rougher filter (1) from of the gas outlet and finer filter (2) from the gas inlet side and clean them with a brush or white spirits. Insert cleaned filters, secure them with space washers and insert a new filter tablet. Screw on the filter housing. NOTE: O-ring (3) do not damage! If the filter housing or a connector is damaged, use new filter housing! Replace the hoses. Flow direction: The Flow direction of the fine filter is marked with an arrow on the filters housing. 39 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 10.5 NOx protection filter (PURAFIL) The NOx filter is to be renewed after discoloration of violet to dark-brown / black. The hoses if necessary clean or replace 10.6 Servicing Acrodisc # 51513 (option) Remove the hoses Change Acrodiscfilter – replaced the hoses. 40 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 10.7 Change the mains fuses If the analyser cannot charge the battery in spite of connecting to mains (no mains indication in the display ), than the fuses ( 3,15 A slow) of mains connector is burn out and has to be replaced! Note: If the fuse will burn out a second time, it is necessary to look for the cause. Hints: 1. The optional heated sample line has a short-cut. 2. The internal switched mode power supply has a short-cut 41 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 10.8 Change the lithium battery for sensor BIAS voltage supply Note: We recommend to let this job be done by a service department ! If it is necessary to replace the BIAS battery earlier than service interval, open the front panel of the analyser (4 hexagon socket screws). Remove the 6 screws and the marked cable (1). Lift the board with the soldered battery and pull it out of the connectors of the complete board. Remove the battery by means of a dissolver pump and insert the new battery (# 11313). After the change of the battery and assembling of the device, the U-BIAS values displayed during the self test should be correct – approx. 3.000 mV. 42 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 10.9 Servicing gas pump # 55513 Remove the hoses, NOTE: Consider installation direction of the hoses! Whether the service of this pump is possible in the inserted condition in RASI, depends on the options of the analyzer If the disassembly of the hose pump is necessary, unscrew the marked fixing screws. At the same time fix the nuts/mothers with an open end wrench on the lower surface of the mounting plate! Unscrew the 4 marked screws by means of a TORX screwdriver size TX10 and remove the cover plate inclusive the rubber sealing. 43 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd Remove the fixing ring (2) of the valve membrane # 11212 (1) by means of a small screwdriver. Renew the valve membrane or clean it with white spirit and replace the fixing ring. Turn the pump head housing on the other side and renew the second valve membrane or clean it with white spirit. In the case of different coating of the valve membrane, the smoothly side is inserted to the valve seat. Set and on the pump attach the rubber seal with metal plate on the pump head housing. The four fixing bolts first strongly tighten and afterwards the screws crosswise tighten, until that the rubber seal straight is not laterally outsqueezed. Replaced the hoses. 44 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 10.10 Servicing CO purging pump # 54151 Diaphragma clean ob renew 45 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 10.11 Servicing CO purge solenoid valve # 59687 Clean channels 46 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 10.12 Replace O2 sensor # 58048A ATTENTION: Sensors can contain acid. Pay attention to security indications for manipulation! In case of a leakage of the sensor, wear protection gloves! The condition of the electro-chemical sensors is checked at every auto-zero cycle. If the sensor is not ok, an alarm message is indicated in the display and system alarm relay will be triggered. The measurement will continue but without O2 measurement. To find out whether a sensor is faulty or not, please pay attention to the chapter 13.1 "service-values"!! Unlock connection cable of oxygen cell (# 58048), unscrew the O2-cell out of the adapter plate mounted on the sensor manifold. The O-ring sealing and the filter paper (# 56872) of the sensor manifold should be changed too! 47 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 10.13 Dismount the gas cooler (RASI (RASI 901 90 1 ) 1) Before you disassemble the gas cooler, you should mark the two parts as shown!! Screw out the four screws, by turning anti clock wise 48 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd Screw out the four screws, by turning anti clock wise Now you can pull up the white housing, it can happen, that the black cylinder will stay in the housing. 49 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd Take out the cylinder and the O-Ring out of the housing Replace the housing if necessary, Insert the O-Ring Insert the cylinder into the housing, there is only one way to fit the cylinder, because of the sensor wire…. Be careful not to break the KTY sensor!! 50 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd In case you just replace the white housing, you use thermolube between the Peltier Element and the cooler block and also between the Peltier Element Aluminium block. IN CASE THAT THERE IS NO THERMO-LUBE BETWEEN THESE TWO PARTS; THEN WE HAVE USED A SPECIAL HEAT TRANSFER FOIL; THIS FOIL CAN BE REUSED IF NOT DAMAGED; OR YOU CAN ORDER NEW HEAT TRANSFER FOIL. (Part Number: 61345) In case you just replace the white housing, you use Thermolube between the Peltier Element and the Cooler block and also between the Peltier Element Aluminium block. Please insure yourself, that you have placed the Peltier Element the correct way. (the red and black wire have to be placed in the same direction as seen on the picture!!!) IN CASE THAT THERE IS NO THERMO-LUBE BETWEEN THESE TWO PARTS; THEN WE HAVE USED A SPECIAL HEAT TRANSFER FOIL; THIS FOIL CAN BE REUSED IF NOT DAMAGED; OR YOU CAN ORDER NEW HEAT TRANSFER FOIL. (Part Number: 61345) 51 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd Just a thin layer of Thermolube Please insure yourself, that you have placed the Peltier Element the correct way. (the red and black wire have to be placed in the same direction as seen on the picture!!!) IN CASE THAT THERE IS NO THERMO-LUBE BETWEEN THESE TWO PARTS; THEN WE HAVE USED A SPECIAL HEAT TRANSFER FOIL; THIS FOIL CAN BE REUSED IF NOT DAMAGED; OR YOU CAN ORDER NEW HEAT TRANSFER FOIL. (Part Number: 61345) Now you can assemble the parts again (the red and black wire have to be placed in the same direction as seen on the picture!!!) You screw in the screws… try to get the same pressure on the springs at the same time. After you have screwed all the 4 screws tight (until the 4 springs are pressed together) you release the screws again for 1,5 turns. 52 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 11 Adjustment Adjustment To select adjustment menu, please access main “Xtras” menu by pressing key Scroll the cursor by means of Press , keys and select the adjustment function. key and analyzer will ask for the PIN code The adjustment menu is protected against use of non-authorized persons by a PIN code. At wrong input of PIN code, the analyser will return to main settings menu. For PIN code ask Service department Adjustment of electrochemical sensors and IRIR -bench see user man manual chapter 8.5 . 11.1 Adjust temperatures temperatures Note: These adjustments are factory made, it is generally not necessary to repeat them! Testtools: 1. Plug with thermo couple short-circuit and adjusted 2KOhm reference 2. 250°C emulator for thermo couple with 2kOhm reference cable , : : select the “Temperatures” menu by moving the cursor enter selected menu (highlighted line) 53 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd In this menu it is possible to correct offset and span errors of the different thermocouple amplifiers: o for combustion air measurement (T-air) o for gas temperature measurement (T-gas) o for cold junction compensation of thermocouples (T-ref) o 11.1.1 Adjust offset of the thermocouple TT- air amplifier 1. Select T-air offset with the cursor 2. connect short-circuit / 2kOhm plug to the T-air socket of the analyzer 3. wait at least 5 minutes 4. press - key = zero 5. the value “T- air span” must be 0.0 (± 0,1) now! 11.1.2 Adjust offset of the thermo couple TT-gas amplifier 1. Select T-gas offset with the cursor 2. connect short-circuit / 2kOhm plug to the T-gas socket of the analyzer 3. wait at least 5 minutes 4. press - key = zero 5. the value “T- gas span” must be 0.0 (± 0,1) now! 11.1.3 Adjust span of the thermo couple T air amplifier 1. The offset of the thermocouple amplifier is already adjusted! (see chapter 11.1.1 and 11.1.1 2. Select T-air span with the cursor 3. connect plug of the 250°C emulator short-circuit / 2kOhm plug to the T-air socket of the analyzer 4. Switch on emulator and set to 250°C 5. wait at least 5 minutes 6. modify the adjust factor by means of , or keys, until the displayed value is 250°C (± 0,3°C) 11.1.4 Adjust span of the thermo couple T gas amplifier 1. The offset of the thermocouple must be adjusted before! (see chapter 11.1.1 and 11.1.1 2. Select T-gas span with the cursor 3. connect plug of the 250°C emulator short-circuit / 2kOhm plug to the T-air socket of the analyzer 4. Switch on emulator and set to 250°C 5. wait at least 5 minutes 6. modify the adjust factor by means of , or keys, until the displayed value is 250°C (± 0,3°C) 54 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 11.1.5 Adjust span of the temperature reference Press .key to access adjustment of T- Ref. , : select T-air / T-gas span 11.1.6 Adjust span of the temperature reference reference TT- air amplifier 1. Select T-air span with the cursor 2. connect short-circuit / 2kOhm plug or 250°C emulator to the T-air socket of the analyzer 3. wait at least 5 minutes 4. modify the adjust factor by means of , , until the displayed value is 0,0°C (± 0,1°C) 11.1.6.1 Adjust span of the temperature reference TT- gas amplifier 1. Select T-gas span with the cursor 2. connect short-circuit / 2kOhm plug or 250°C emulator to the T-gas socket of the analyzer 3. wait at least 5 minutes 4. modify the adjust factor by means of , , until the displayed value is 0,0°C (± 0,1°C) Final check: If all 3 steps described before are accomplished, then the measured values must show the following values: With short-circuit 2kOhm plug: With 250°C emulator : 0,0°C (± 0,2°C) 250,0°C (±0,5°C) 55 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 11.2 Adjust Pressure Note: These adjustments are factory made, it is generally not necessary to repeat them! : activate pressure adjustment : end: return to adjustment menu Test tools: Pressure calibrator Manual calibration: After setting the zero point at the pressure calibrator, the adjustment pressure is carried out in two steps: : zero: set value to zero 11.2.1 Adjustment of the lower range The pressure at the reference device will be changed up to approx. - 10 hPa, hPa however not more as 20 hPa. Following the pressure factor of the display has to be modified by means of the corresponds to the value of the reference device. , - keys until the displayed value 11.2.2 Adjustment of the upper range The pressure of the reference device will be raised still the displayed value is approx. 90 hPa, however no less than 80 hPa. If the displayed value is smaller, it is not possible to correct them. Following the pressure factor of the display has to be modified by means of the value corresponds to the value of the reference device. : end: end return to adjustment menu 56 , - keys until the displayed START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 11.3 AUX channel adjustment Note: These adjustments are factory made, it is generally not necessary to repeat them! The analog input (AUX) allows user to data log an additional thermocouple or transmitter with voltage output signal (0-10V) or current signal (0/4-20mA). , : select the line “AUX-channel” Adjustment menu AUX channel : activate AUX channel adjustment AUX input adjustment , : select the item , : set the factor of the selected item : zero: set value to zero .: not active : modify: modify the values : not active : end: return to adjustment menu 57 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 11.3.1 Adjustment thermocouple AUX amplifier Connect to AUX socket the calibrator, turn switch for zeroing ( pos. 1), select line “ AUX offset” and press key to set to zero the amplifiers offset. Turn switch to position 2 (thermocouple voltage) , select line “T-AUX span” and adjust the span factor of thermocouple amplifier with keys , . Temperature value must show: +250°C for 10,151 mV ( K type thermocouple ) +500°C for 20,64 mV ( K type thermocouple ) Select line “ T-ref span” and compare value of the cold junction compensating sensors for the thermocouples with a reference temperature device ( e.g. a precision glass thermometer). Adjust the factor to have the same temperature displayed as the reference thermometer. 11.3.2 Adjustment 00 -10V AUX Connect to AUX socket the calibrator , turn switch for zeroing ( pos. 1), select line “ AUX offset” and press key . Turn switch to position 3 ( 10,00 V) , select line „V span“ and adjust the span factor with keys reading on the display. , for 10V , for 20mA 11.3.3 Adjustment 44 -20mA Connect to AUX socket the calibrator , turn switch for zeroing ( pos. 1), select line “ AUX offset” and press key . Turn switch to position 4 ( 20mA) , select line „mA span“ and adjust the span factor with keys reading on the display. 58 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 11.4 Analog output (4 - 20mA) Note: These adjustments are factory made, it is generally not necessary to repeat them! This function allows user to calibrate the analog current output. , : : select the line “Analog output (4-20 mA)” activate analog output adjustment , : select the output channel (1 to 8) , : select Offset 4 mA or 20 mA Test tools: Digital multimeter. Test plug with 100 Ohm resistors, 0,1% tolerance, for each of the 8 channels. Manual calibration: Connect the test plug to the analog output socket of the analyzer. Measure with the digital multimeter the voltage above the resistor of the selected output channel. 100 Ohm resistor measured voltage 0,4 V 4 mA value at the display: 4,00 100 Ohm resistor measured voltage 2,0 V 20 mA value at the display: 20,00 , : adjust the output until on the digital multimeter 4,00 is displayed for 4 mA and 20,00 for 20 mA return to adjustment menu 59 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 12 Service maintenance plan A check of the analyser at our service department is recommendable: • after 1000 working hours • if the last check of the analyser was effected 11 month ago. As soon this period is exceeded, the analyser displays 2 times after switching on: This message can be skipped by pressing the - key. For more information’s about the service plan, please call our service department. 13 Self diagnosis The analyser is equipped with a self-diagnosis program. All internal functions are monitored and displayed if necessary. Switch on analyser: Error message: all values are checked In the “Menu” e. g. “NO sensor not OK / analyser not ready for measurement” is displayed. Measuring analyser can be activated in all menus except for menu “Measurement” (measurement cannot be started). Service program: 13.1 Serrvice. The mV In case of an error message, change to the Extra Menu and select Se values of e. g. the sensors, the flue gas temperature sensitive element etc. are displayed. Afterwards, the mV values are indicated, which restrict the “OK” range: range Sensors: ( to fresh air ) O2 sensor : CO sensor : CO sensor^(H2 compensated CO sensor up to 100.000 ppm SO2 sensor : NO sensor : NO2 sensor : H2S sensor: H2 sensor: 13.2 +200 mV up to + 500 mV -13 mV up to + 25 mV -35 mV up to + 50 mV -13mV up to + 25 mV -13mV up to +25mV -13mV up to +25mV -13mV up to +25mV -13mV up to +25mV -13mV up to +25mV Battery voltage Battery according to state of charge: Battery fully charged 13.000mV = 13V (voltage) Warning limit (the battery symbol on the dis11.100mV = 11,1V (voltage) play starts flashing) Cut off limit of the analyser, protection against 10.500mV = 10,5V (voltage) total discharge 60 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 13.3 Temperatures TH Gas: (thermo element gas) -500mV to +500mV with room temperature: app. 0mV KTY Gas: (refer. temperature gas) -500mV to +500mV with room temperature: app. 200mV TH Air: (thermo element air) -500mV to +500mV with room temperature: app. 0mV KTY Air: ( refer. temperature air) -500mV to +500mV with room temperature: app. 200mV KTY Sensor ( temp. of sensor): 0 to 5000mV room temperature: app. 2000mV ( Appendix 1: chart in mV regarding temperature in °C ) 13.4 Draft Draft: -500mV to 500mV not pressurized: -20 mV to + 20mV 13.5 BiasBias -voltage Bias: (indication of bias voltage) +2.999mV to + 3.250mV If the above mentioned values are exceeding the allocated ranges, a defect is present. If no sensitive elements are connected, the corresponding fields in the service print are marked with - - - - - ( negative service value) or with + + + + + (positive service value ). 13.6 KTYKTY- chart AD [ mV ] T [ °C ] 13.7 163 0 170 5 177 10 185 15 192 20 200 25 208 30 216 35 225 40 233 45 242 50 5 10 15 20 25 30 35 40 45 50 PT2000PT2000- chart AD [ mV ] T [ °C ] 0 Scroll service data: Activate printer with: , and , . print of the current service data, analyser number, EPROM version number Note: The number of prints can be determined by pressing the printer key (e. g. pressing printer key twice = 2 prints). Quit service program: get back to Extra Menu with key 61 . START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 14 Appendix 14.1 Manual for firmware update of H8H8 - Industrial analyzers 14.1.1 System requirements • Operating system MS Windows 98SE/ME/2000/XP or later • Pentium PC 450MHz or better • One avalable RS232 port. It should be a real RS232 port. A RS232-USB adaptor may work, but may fail as well. 14.1.2 Important Important hints and warnings • Most probably stored measurements and sites get lost during a firmware update! • After the update the analyser must be switched off, as soon as it has reached the self test window! Please disconnect mains (unplug cable or switch off the master switch), analysers with battery additionally need to be switched off by pressing the keys F1 and F4 simultaneously. Now you can restart the analyser and use it with its new firmware. • Please start the update only with a reliable mains connection. 14.1.3 Update procedure • Please do not switch-on the analyser yet and disconnect mains! Connect the analyser with a 0-modem-cable (at least five-wire crossed) to the PC’s RS232 port. • Start the PC-program “MRU_UPLOADER.EXE”. • Select the COM-port, which is connected with the analyser by clicking on “RS232” and then on the appropriate “COMx”. • Load a firmware file by clicking on “file” / “load file” and selecting a file. • Now press and hold down the F1 key and connect mains (plug cable or switch on the master switch). Hold the F1 key down until the PC indicates the message “MRU unit (H8-generation) recognized”. Now you can release the F1 key. • The update usually takes less than one minute. The unit’s display stays empty during the uploading process. When the update has finished, the unit starts its program as usual. Please bear in mind now the important hints and warnings written above concerning switching-off and data loss! 14.1.4 Possible causes and solutions in case of update failure: • Cable problems: cable defective, wrong cable or cable not properly plugged • Another software runs on the used PC reserving the selected RS232 port: Close all running programs and restart MRU_UPLOADER.EXE. • A serial mouse uses the one and only RS232 port: Use another PC or another mouse. • You have not selected the COMx port which is connected to the analyser: Change the COM-port selection. 62 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 14.2 Electrical connections 14.2.1 Analog output All 8 analog outputs are user settable. For this, all measured and calculated values can be used. ! The analog outputs have no galvanic isolation ! 14.2.2 RS 232 connector - + Pin 9 leads a voltage of ( +5V ) to supply external units ( for example a Bluetooth module for wireless data transfer). 14.2.3 RS 485 connector This connector is used only for supply and data transfer to external smart transmitters ( e.g. TOM420 ). 63 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 14.2.4 RS 485 converter connection to PC Connection RASI 901 to RS 485 converter SWG 300300 -1 R+ RTT+ GND (housing) RS 485 converter 1 = T+ 2 = R3 = T4 = T+ GND not connected Switch settings at the converter: SW1 = DCE SW2 = T ON/ R ON Max. length of transmission cable: 1.000 m with screened cable The screen has to be connected at the PE mounting at the PC housing. 64 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd SWG 300300 -1 R+ RTT+ GND (housing) RS 485 converter 1 = T+ 2 = R3 = T4 = T+ GND not connected Switch settings at the converter: SW1 = DCE SW2 = T ON/ R ON Max. length of transmission cable: 1.000 m with screened cable The screen has to be connected at the PE mounting at the PC housing. 65 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 14.2.5 RS 232 connection to PC RS 232 cable from analyzer (RS232) to PC (COM/RS232) length # 3m 60003 5m 51532 10 m 51562 20 m 54367 66 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 14.3 Transmission Transmission protocol 14.3.1 Online data transmission protocol 67 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 14.3.2 data storage transmission protocol 68 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 14.4 Display messages Message 0 SET TO ZERO, LAUNCHED Message 1 Analyser configuration is being saved Message 2 Set to zero in progress Message 3 ?? SENSORS ?? ? NOT READY ? Message 4 SET TO ZERO FINISHED, SENSORS READY, ANALYSER READY FOR MEASUREMENT Message 5 MEASUREMENT VALUES STORED Message 6 DATA STORAGE FULL Message 7 NO MEASUREMENT VALUES STORED Message 8 “not used” Message 9 ZERO SETTING DRAFT SENSOR PLEASE WAIT Message 10 “not used” Message 11 CO-SENSOR not ok! Limited measurement Message 12 H2-SENSOR not ok! Limited measurement Message 13 NO-SENSOR not ok! Limited measurement Message 14 O2-SENSOR not ok! Limited measurement Message 15 REMINDER! PLEASE RECHARGE THE BATTERY PERIODICALLY! Message 16 This fuel type is currently selected for measurements. Therefore it can’t be disabled. Message 17 -Attention- Administrator PIN-Code is 6xF1! PIN-Codes are disabled! Message 18 69 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd !! CAUTION !! TRANSMISSION WAS NOR SUCCESSFUL Message 19 -CONNECTION INTERRUPTED – WRONG PC-COM SELECTED – WRONG CABLE – PC-RECOURCES CONFLICT Message 20 DATA TRANSMISSION FROM PC WAS SUCCESSFUL Message 21 PC NOT READY Message 22 CUSTOMER’S MEMORY IS FUL Message 23 DATA TRANSMISSION TO PC WAS SUCCESSFUL Message 24 BATTERY LOAD INSUFFICIENT FOR PRINT-OUT CONNECT MAINS CABLE Message 25 “not used” Message 26 “not used” Message 27 ANALYSER –ERROR POSSIBLE LOSS OF TIME/DATE AND STORED DATA Message 28 MEASUREMENT STOPPED Message Messag e 29 MEASUREMENT STARTED Message 30 !!! ERROR !!! POSSIBLE LOSS OF CONFIGURATION DATA Message 31 SEARCH WITHOUT SUCCESS Message 32 NDIR bench not ready! Limited measurement Message 33 DRAFT/PRESSURE WILL BE SET TO ZERO ALL NOZZLES PRESSURELESS? Message Mes sage 34 !! CAUTION !! DUE FOR SERVICE CONTACT YOUT LOCAL DEALER Message 35 Configuration transmission error! Configuration rejected! Message 36 DATA TRANSMISSION IN PROGRESS PLEASE WAIT 70 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd Message 37 A new customer was created. Message 38 Sensors are not rinsed yet. Message 39 Automatic zeroing Please wait… 71 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 14.5 Lists of countries and fuel types 14.5.1 General information O 2 max = 20.96% O2 content O 2 = measured O2 value [%] O2bez = O2-reference value [%] (fuel specific) CO 2 max = CO2max-value [%] (fuel specific) V AG min, tr = Flue gas volume, dry and O2-free (fuel specific) H u , n = calorific value , normality (fuel specific) 14.5.1.1 CO2, Lambda, losses, efficiency O2 CO 2 = CO 2 max ⋅ 1 − O 2 max λ= CO 2 max O 2 max = CO 2 O 2 max − O 2 (prefer the 2nd O2 formula!) A2 losses = (T fluegas − Tair ) ⋅ + B (temp. in °C, A2 and. B fuel specific) O 2 max − O 2 efficiency = 100% − losses 14.5.1.2 Dew point (after DIN 4705, part 1, page 17) tP = tP pD pL 4077,9 − 236,67 23,6448 − ln ( p D ) : dew point temp. in °C : steam part. pressure : atmospheric pressure with fW CO2 pD = H 2O * pL 100 with H 2O = 1,1 + 100 f 1+ W CO 2 H2O : water vapour content [%] : humidity value of fuel [%] : carbon dioxide content [%] At standard pressure (1013 mbar) the dew point is calculated: 4077,9 4077,9 tP = − 236,67 = − 236,67 100 100 23,6448 − ln 1,1 + − ln (1013) 16,7241 − ln 1,1 + fW f 1+ 1+ W CO 2 CO 2 14.5.1.3 COCO- conversion of CO [ppm] COunv[ ppm] = CO[ CO[ ppm ] = CO[ ppm] ⋅ λ 0%O 2 ppm O 2 max − O 2bez ] = CO[ ppm] ⋅ O 2bez O 2 max − O 2 72 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd mg ] = CO[ ppm] ⋅ 1,249 m3 CO[ mg / m 3 mg O 2 max − O 2ref CO[ ] = CO[ 3 ] ⋅ O 2ref O 2 max − O 2 m V AG min, tr mg mg / m 3 V AG min, tr mg ] = CO[ ]⋅ = CO[ 3 ] ⋅ λ ⋅ kWh 0%O 2 H u ,n H u ,n m CO[ mg ]= MJ CO[ mg ] kWh 3,6 CO[ 14.5.1.4 NONO- conversion of NO [ppm] [pp m] NOundel [ ppm] = NO[ ppm ] = NO[ ppm] ⋅ λ 0%O 2 NO[ ppm O 2 max − O 2ref ] = NO[ ppm] ⋅ O 2ref O 2 max − O 2 NO[ mg ] = NO[ ppm] ⋅ 1,339 m3 NO[ mg / m 3 mg O 2 max − O 2ref ] = NO[ 3 ] ⋅ O 2ref O 2 max − O 2 m NO[ V AG min, tr mg mg / m 3 V AG min, tr mg ] = NO[ ]⋅ = NO[ 3 ] ⋅ λ ⋅ kWh 0%O 2 H u ,n H u ,n m NO[ NO[ mg ]= MJ mg ] kWh 3,6 NO[ ppm O 2 max − 1,8% ] = NO[ ppm] ⋅ 14%CO 2 O 2 max − O 2 14.5.1.5 NO2NO2- conversion of NO2 [ppm] No conversions of NO2!. All the values of interest are in the NOx conversion. 14.5.1.6 NOxNOx- conversion of NO [ppm] (possible also of NO2 [ppm]) NOx[ ppm ] = NO[ ppm ] ⋅ 1,05 (if no NO2-sensor exists) NOx[ ppm ] = NO[ ppm ] + NO 2[ ppm ] (if a NO2-sensor exists) NOx undel [ ppm] = NOx[ NOx[ ppm ] = NOx[ ppm] ⋅ λ 0%O 2 ppm O 2 max − O 2ref ] = NOx[ ppm] ⋅ O 2ref O 2 max − O 2 If NOx is specified in mg, it has to be considered, that all the NO in the atmosphere will become to NO2. Therefore the conversion factor ppm => mg is factor of NO2. mg NOx[ 3 ] = NOx[ ppm ] ⋅ 2,053 m 73 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd NOx[ mg / m 3 mg O 2 max − O 2ref ] = NOx[ 3 ] ⋅ O 2ref O 2 max − O 2 m NOx[ V AG min, tr mg mg / m 3 V AG min, tr mg ] = NOx[ ]⋅ = NOx[ 3 ] ⋅ λ ⋅ kWh H u ,n H u ,n 0%O 2 m mg NOx[ ]= MJ mg ] kWh 3,6 NOx[ ppm O 2 max − 1,8% ] = NOx[ ppm] ⋅ NOx[ 14%CO 2 O 2 max − O 2 14.5.2 Fuel type list Great Britain Some analyzer disposes only of a subset of this list. England Fuel type Test gas Oil light Oil heavy Nat. gas heavy Nat. gas light Nat. gas H blow Nat. gas L blow Coal gas Coal gas blow Coal Wood dry CO2max 0,0 15,3 15,8 11,7 12,2 11,7 12,2 10,0 10,0 19,1 19,4 A2 0,00 0,68 0,66 0,66 0,63 0,66 0,63 0,73 0,73 0,65 0,65 B 0,000 0,007 0,007 0,009 0,009 0,009 0,009 0,011 0,011 0,009 0,009 Fuel type lists for further countries on demand! Data subject to change without notice! Date of issue: 20110530 74 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd 75 START-UP AND SERVICE MANUAL RASI 900 / RASI 901 EiUK Eurotron Instruments (UK) ltd Technical change without notice! English Date of issue: 20110530 76