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TABLE OF CONTENTS CHAPTER 1: INTRODUCTION Freeze Dry Process Freeze Dry Rates Freeze Dry Capacity Samples Containing Volatile Substances About This Manual Typographical Conventions Your Next Step 1 1 2 3 4 4 6 6 CHAPTER 2: PREREQUISITES Electrical Requirements Location Requirements Vacuum Pump Requirements Chamber or Manifold Requirements 7 7 8 8 9 CHAPTER 3: GETTING STARTED Unpacking Your Freeze Dryer Freeze Dryer Components Setting Up Your Freeze Dryer Component Orientation Vacuum Pump Connection Electrical Connection Chemical Resistance of Freeze Dryer Components Solvent Safety Precautions 10 10 11 12 12 13 13 13 15 CHAPTER 4: USING YOUR FREEZE DRYER Freeze Dryer Controls Operation Checklist Vacuum Pump Ballast Setting Operating the Freeze Dryer Set-Up Automatic Start-Up Manual Start-Up Setting the Operating Vacuum Level Pre-Freezing Samples Adding Sample 17 18 19 19 20 20 22 22 23 24 24