Download Developing a Guided Procedure for Troubleshooting HPLC and
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ooting solution is phic es run with lected reference s electronic ystem within a preprogrammed tion of the Electronic ware tools ng solution. area of the 25% for impurity B (Figure 3, Peak 1, bottom) compared to the in spec result of 0.03%. FIGURE 3. Out-of-spec result in impurity analysis. 1.6 AU 2 1 1 0 0.9 AU 3 In spec result 2 3 4 4 min Out-of spec result 2 1 00 RS system PG-3400RS, tat TCC-3000RS Solution (PN mn (Thermo m, 4 m , PN XPert gradient 0 min 0.5 0.25 0 The interpretation of the result is performed according to the methodical troubleshooting workflow of Fig. 4. FIGURE 4. Troubleshooting workflow. Install XPert column, load standards and eWorkflow, mobile phase (U)HPLC results questionable e package SR1. Run isocratic or gradient method => immediately review tips in report Test fails Test passes Review all details of XPert report applying system and system setup troubleshooting, rerun XPert, if recommended: perform maintenance or repair Run XPert standards with original column, modify method accordingly (method transfer tools) /v) rate min 95% B, 4.5– Test fails Initiate Instrument Service rate ogram. 5 ogram. 8 9 4.0 min 4.5 Test passes Perform validation or SST according to your SOPs, rerun XPert to benchmark application & system Test fails Replace column min 4.0 After replacing the colu the operability of the co The interpretation of the impurity can be assess Step IV – Performance Long term monitoring o indicators is implement periodically running the column allowing an ear done without exporting settings of the XPert Tr FIGURE 8. Using Chro functionality for perfo Test passes Investigate application and verify sample or standard preparation Step I – System Check: First the isocratic test mix is separated on the reference column by easy method installation using the eWorkflow. The results are immediately assed by an report, showing that the system is in an operable status( Fig. 5) FIGURE 5. Automatically evaluated parameters show operable system. 10 Step III – Replacing th Conclusion an • A standardized check reference test mixture chromatographic para troubleshooting indepe • Automatically evaluat provide helpful indica suggested actions to simplified for LC begi knowledge and practi while making the use and introducing perfo intervention if things g Thermo Scientific Poster Note • PN71313-ISC-EN 0914S 5 • The XPert troublesho