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12
Put the working electrode with its active layer
downside on top of the T-frit
13
Place the appropriate spacer disc on top of the WE
(SS 316L for aprotic, gold for aqueous
electrolytes).
NOTE: Three different spacer discs (thickness 2.1,
2.2 and 2.3 mm) are provided to initially adjust the
membrane for a given WE thickness close to its
neutral (flat) position (see sketch below). Use the
2.3 mm disc for a sample thickness between 0 and
150 µm.
WE
Spacer disc
Metal membrane
T-frit
CE
Page 12 of 31
ECD-nano_manual / 27/02/2015