Download Magnetic Property Measurement System
Transcript
C H A P T E R 7 System Operations 7.1 Introduction This chapter contains the following information: 7.2 • Section 7.2 explains how to set the system temperature. • Section 7.6 explains how to monitor helium transfers. • Section 7.3 explains how to set the magnetic field. • Section 7.7 explains how to make the MPMS enter standby mode. • Section 7.4 explains how to control the atmosphere in the sample chamber. • Section 7.8 explains how to perform several advanced system operations. • Section 7.5 explains how to tune the SQUID. Setting the Temperature 1. Do one of the following: (a) select Instrumenth Temperature or (b) click on any temperature status panel in the status bar. The Temperature Parameters dialog box opens. The dialog box indicates the status of the temperature and includes temperature control commands. 2. Specify the new temperature set point. The state of the MPMS and the maximum system temperature limit the maximum temperature you can specify. 3. Specify the rate at which the MPMS attempts to ramp to the set point. For systems without the Enhanced Temperature Control (ETC) option, you can specify the use of Temperature Undercool. 4. Figure 7-1. Temperature Select Set. The temperature immediately begins to ramp Parameters Dialog Box to the set point. The system monitors the changing temperature and temperature status. The Temperature Parameters dialog box and the temperature status panels display the temperature and status. If a sequence runs while the Temperature Parameters dialog box is open, the Status panel in the dialog box indicates the status of any Set Temperature or Scan Temperature commands that are executed as part of the sequence. Quantum Design MPMS MultiVu Application User’s Manual 7-1