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Appendix E: Maintaining High-performance Liquid Nitrogen Dewars. Re-Pumping the Dewar The symptoms that indicate the dewar needs to be re-pumped are: • • • The liquid nitrogen temperature indicated by the software as being the SINK temperature should normally be approximately -190C. The CCD temperature is usually much higher, approximately -120C. If the vacuum starts to degrade then the CCD temperature will be seen no longer to reach as low a level as it normally does because of the greater losses associated with the poor vacuum. The length of time for which a single fill of liquid nitrogen lasts before the dewar needs to be re-filled will be noticed to progressively decrease. Condensation forms on the outside of the dewar or the dewar feels cold and clammy to the touch. Should condensation occur, and it can occur particularly on the front window of the dewar, then this may be an indication that the vacuum needs to be improved. Remember, however, that no matter how good a liquid nitrogen dewar is, under conditions of high humidity, condensation will occur. It is inevitable that one of the coldest parts of any liquid nitrogen dewar will be the window that protects the CCD from the outside world. As a result of high humidity conditions obtaining then it is quite likely that problems will arise because of condensation on the window. If this is a serious problem for example because the unit is being used on a telescope in a cold, damp, climate then it is sometimes helpful to arrange that dry nitrogen gas (possibly from the boil-off from the nitrogen inside the liquid nitrogen dewar) is directed with a small tube onto the front window of the dewar. In practice most dewars will need to be re-pumped occasionally, depending on usage. Equipment Required A vacuum pumping system such as a turbo molecular pumping system or a vapour diffusion pumping system. Each should be able to achieve a vacuum of 2x10 -7 mbars or better. You really need to have a vacuum pumping system with associated vacuum gauges and gauge heads. Suitable vacuum piping and vacuum connectors must also be provided. Warning: never use an ion pump or a sputter-ion pump as they can cause irreparable damage to static sensitive CCDs. The dewar contains a sorb pump whose function is to remove the remaining gas molecules once the dewar has been pumped and the valve closed. It operates by adbsorbing free gas molecules when cold. If the dewar is cold when being pumped with an external vacuum pump, air in the space above the diffusion pump and oil from the diffusion pump may be drawn into the dewar. This oil will contaminate the sorb pump and the face of the CCD and will be almost impossible to remove, leaving the dewar and the CCD chip within it irreparably damaged. The liquid nitrogen filled dewar is a much more powerful pump than the diffusion pump so pumping the dewar when cold may actually be worse than not pumping the dewar at all. Page 69