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Contents
1.
INTRODUCTION ..................................................................................................................... - 1 1.1
HARDWARE SPECIFICATIONS ........................................................................................................... - 1 -
1.2
ELECTROCHEMICAL SIGNAL GENERATOR ............................................................................................ - 2 -
1.3
FRONT PANEL .............................................................................................................................. - 2 -
1.4
POTENTIOSTATIC MODE ................................................................................................................. - 3 -
2.
INTRODUCTION ..................................................................................................................... - 4 2.1
SYSTEM REQUIREMENTS ................................................................................................................ - 4 -
2.2
SOFTWARE INSTALLATION............................................................................................................... - 5 -
3.
MENU .................................................................................................................................... - 5 3.1
FILE ........................................................................................................................................... - 6 -
3.2
EDIT .......................................................................................................................................... - 6 -
4.
SYSTEM SETUP....................................................................................................................... - 7 4.1
COM PORT SETUP ........................................................................................................................ - 7 -
4.2
TIMING MEASUREMENT ................................................................................................................ - 7 -
4.3
RESET WORKSTATION .................................................................................................................... - 7 -
5.
EXPERIMENT SETUP............................................................................................................... - 8 5.1
CELL& ELECTRODE SETUP .............................................................................................................. - 8 -
5.2
PSTAT/GSTAT SETUP ..................................................................................................................... - 9 -
5.3
WAITING BEFORE RUN ................................................................................................................. - 10 -
6.
STABLE POLARIZATION ........................................................................................................ - 10 6.1
OPEN CIRCUIT POTENTIAL ............................................................................................................ - 10 -
6.2
POTENTIOSTATIC ........................................................................................................................ - 11 -
6.3
GALVANOSTATIC ......................................................................................................................... - 13 -
6.4
POTENTIODYNAMIC .................................................................................................................... - 15 -
6.5
GALVANODYNAMIC ..................................................................................................................... - 17 -
7.
TRANSIENT POLARIZATION .................................................................................................. - 18 7.1
MULTI-POTENTIAL STEPS ............................................................................................................. - 18 -
7.2
MULTI-CURRENT STEPS ............................................................................................................... - 19 -
7.3
POTENTIAL STAIR-STEP ................................................................................................................ - 21 -
7.4
GALVANIC STAIR-STEP ................................................................................................................. - 22 -
8.
VOLTAMMETRY.................................................................................................................... - 23 8.1
LINEAR SWEEP VOLTAMMETRY ...................................................................................................... - 23 -
8.2
CYCLIC VOLTAMMETRY ................................................................................................................ - 24 -
8.3
STAIRCASE VOLTAMMETRY............................................................................................................ - 27 -
8.4
SQUARE WAVE VOLTAMMETRY ..................................................................................................... - 28 -
8.5
DIFFERENTIAL PULSE VOLTAMMETRY .............................................................................................. - 29 -
8.6
NORMAL PULSE VOLTAMMETRY .................................................................................................... - 31 -