Download User Guide: Liquids NMR

List of Figures
Figure 41. HMQC Pulse Sequence, Showing Movement of Attached Protons ..........................
Figure 42. Evolution Time Added Between X-Nucleus Pulses ..................................................
Figure 43. HMQC with BIRD Pulse Nulling Effects .................................................................
Figure 44. Basic HMQC Pulse Sequence ...................................................................................
Figure 45. Normal 13C Spectrum of 13CH3I ...............................................................................
Figure 46. Normal 1H Spectrum of 13CH3I ................................................................................
Figure 47. HMQC Without and With X-Nucleus Pulses ............................................................
Figure 48. Calibration of pwx, Coarse and Fine ........................................................................
Figure 49. HMQC 4-Pulse Cancellation without 2H Bandpass Filter ........................................
Figure 50. HMQC 4-Pulse Cancellation with 2H Bandpass Filter .............................................
Figure 51. HMQC Without and With 13C Decoupling ...............................................................
Figure 52. Coupled HMQC Spectrum of 13CH3I .......................................................................
Figure 53. Verifying Cancellation with pwx=0,90 ..................................................................
Figure 54. Optimizing the BIRD Nulling Time ..........................................................................
Figure 55. Coupled HMQC Spectrum of 3-Heptanone ..............................................................
Figure 56. Expansion of Coupled 3-Heptanone HMQC Showing Multiplets ............................
Figure 57. Decoupled HMQC Spectrum of 3-Heptanone ..........................................................
Figure 58. Display of Regression Fittings (expl Program) .........................................................
Figure 59. Temperature Control Window ...................................................................................
Figure 60. Carousel Autosampler Carousel and Driver ..............................................................
Figure 61. Carousel with Sensor Arm in Locked and in Run Positions .....................................
Figure 62. Lock Pin on Sensor Arm Disengaged and Engaged ..................................................
Figure 63. Bottom View of Carousel, Showing Connector and Groove .....................................
Figure 64. Optical Sensor and Proper Sample Floating Height ..................................................
Figure 65. Sample Entry Form Window for the Carousel Autosampler .....................................
Figure 66. Manually Loading and Unloading Samples Through Position 1 ..............................
Figure 67. SMS Autosampler .....................................................................................................
Figure 68. Sample Entry Form Window (100 samples) for the SMS Autosampler ...................
Figure 69. NMS Window ............................................................................................................
Figure 70. Sample Entry Form Window for the NMS Autosampler ..........................................
Figure 71. Sample Status Window (status Program) .............................................................
Figure 72. Locate Window (status Program) .........................................................................
Figure 73. Sample Entry Form Window for Walkup Operation .................................................
Figure 74. Gilson 215 Liquid Handler ........................................................................................
Figure 75. VAST Sample Entry Form Window (enter program) ................................................
Figure 76. LC-NMR Pane for VAST ..........................................................................................
Figure 77. VAST Sequence Pane ................................................................................................
Figure 78. VAST Pane ................................................................................................................
Figure 79. VAST Acq & Obs Pane .............................................................................................
Figure 80. VAST Sequence Pane and Frequency Suppression Options .....................................
Figure 81. Partial doneQ File ....................................................................................................
Figure 82. Queue Name and Scout Directory Fields ..................................................................
Figure 83. plate_glue Window and e4x4 glue order. .........................................................
Figure 84. Array of 1D Spectra from a VAST Data Set .............................................................
Figure 85. Plot of a Subset from a 96-Well Sample Plate ..........................................................
Figure 86. Contour Plot of a VAST Data Set ..............................................................................
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VNMR 6.1C User Guide: Liquids NMR
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