Download HPLC
Transcript
12 Injection Port 12.5 Split/Splitless Injection System 12.5.5 Pressure program You can set a program to increase and decrease the column inlet pressure during analysis. If high-boiling point contaminants are clunting shorlty after the target compounds, a pressure program can be used so that the oven temperature does not need to be set higher than necessary. This prolongs column service life. 12.5.5.1 Screen description Select [Press Prog] (PF menu) from the [FLOW] key main screen when the control mode is set to “PRESS,” to display the carrier press screen shown in Fig. 12.5.7 appears. Up to 7 ramps of pressure increase or decrease can be set. Fig. 12.5.7 Pressure program setup screen 12.5.5.2 Parameter list PRESS Range: 0.0−970.0 kPa (Refer to Fig. 3.5.1.), Default: 100 kPa Set the initial pressure and the final pressure for each stage of the pressure program. TIME Range: 0.0−9999.99 min, Default: 1.00 min Set the hold time for the initial pressure and the final pressure for each stage of the pressure program. RATE Range: END/-400.00−400.00 kPa/min, Default: END Set the pressure program rate. If you set the rate to “0”, “END” appears and the program finishes at the previous ramp. If you move the cursor to “END” and set any numeric value other than “0”, the pressure and the time for that ramp can be enterd. NOTE 132 The pressure increase/decrease program rate control range may be limited depending on the total flow rate setup value, the column in use and the purge flow rate. GC-2010