Download Manual - Equipco
Transcript
Method Development 3. Press Exit to close the box. Press Enter Menu to close the menu. 4. Press Enter Menu, SETUP, CONFIG, METHOD, ∫METH, and AUTO. 5. Use the arrow keys to select on and press Enter Menu. Press Exit to close the box. 6. Press Enter Menu, DISPLAY, GC, GRAPH and REINT. The signal will be re-integrated using the new integration settings. 7. Press DISPLAY, GC, PEAK to see if the peaks have been integrated accurately. 8. If you need to change the settings for the other two columns, repeat this procedure for each column. 9. When you have changed the settings for each column, enable all the columns required for your method. Integrator Delay The integrator delay is used to delay the start of integration after the analysis begins. It is used to prevent integration of peaks which may appear as a result of pressure changes during sample injection, especially when large syringe injections are made. If you have more than 25 peaks in an analysis, integrator delay may be used to determine which 25 peaks will be identified. If you are interested in the peaks in the middle or at the end of the chromatogram, set the integrator delay so that the first peaks are not integrated. 1. Press Enter Menu, SETUP, CONFIG, COLUMN. 2. Select the column for which you want to alter the integration settings. Disable the other columns. 3. Press Exit to close the box. Press Enter Menu to close the menu. 4. Press Enter Menu, SETUP, CONFIG, METHOD, ∫METH, and DELAY. 217
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