Download Solid State NMR: AVANCE Solids User Manual - Pascal-Man
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Contents 5.4 5.5 5.6 6 6.1 6.2 6.3 6.4 6.5 7 7.1 7.2 7.3 7.4 8 8.1 8.2 8.3 9 9.1 9.2 9.3 Basic CP-MAS Experiments ..............................................61 Introduction ...................................................................................... 61 Pulse Calibration with CP ............................................................. 61 Total Sideband Suppression TOSS ................................................... 62 SELTICS .......................................................................................... 66 Non-Quaternary Suppression (NQS) ................................................ 69 Spectral Editing Sequences: CPPI, CPPISPI and CPPIRCP ............. 72 FSLG-HETCOR ..................................................................75 Introduction ...................................................................................... Pulse Sequence Diagram for FSLG HETCOR ................................... Setting FSLG HETCOR Experiments ................................................ Results ............................................................................................ 75 76 77 81 Modifications of FSLG HETCOR .......................................83 Carbon Decoupling During Evolution ................................................ 84 HETCOR with DUMBO, PMLG or w-PMLG, Using Shapes ................ 85 The Sequence pmlghet ................................................................. 85 w-pmlghet .................................................................................... 88 edumbohet ................................................................................... 89 dumbohet ..................................................................................... 90 HETCOR with Cross Polarization under LG Offset ............................ 91 RFDR .................................................................................93 9.4 Experiment ...................................................................................... 94 Set-up .............................................................................................. 94 Data Acquisition ............................................................................... 95 Set-up 2D Experiment .................................................................. 95 Spectral Processing ......................................................................... 96 10 Proton Driven Spin Diffusion (PDSD) ...............................99 10.1 10.2 10.3 10.4 10.5 11 11.1 11.2 11.3 4 Possible Approaches for non-13C Samples ...................................... 57 Hints, Tricks, Caveats for Multi-nuclear (CP-)MAS Spectroscopy ...... 58 Setup for Standard hetero-nuclear Samples 15N, 29SI, 31P ............. 58 Pulse Sequence Diagram ............................................................... 101 Basic Setup .................................................................................... 101 2D Experiment Setup .................................................................. 101 Acquisition Parameters .................................................................. 103 Processing Parameters ............................................................... 104 Adjust the Rotational Resonance Condition for DARR/RAD ............ 104 Example Spectra ............................................................................ 106 SUPER ............................................................................. 109 Overview ........................................................................................ 109 Pulse Program ............................................................................... 110 Experiment Setup .......................................................................... 110 Experiment setup ....................................................................... 110 Setup 2D Experiment ...................................................................111 BRUKER BIOSPIN User Manual Version 001