Download User Guide: Liquids NMR

Transcript
Index
V
W
Valco valve
connecting air tubing, 342
variable temperature, See VT
Varian LC-NMR system, 401
VAST
air connections, 343
autosampler, 267, 355
data analysis, 337
files that control operation, 363
Hardware installation and configuration, 341–
362
interface to VNMR, 355
microtiter plate, 337
multiple frequency suppression options, 319
Operation and data processing, 311–341
sample entry form window, 315
sequence pane, 317
set up NMR experiments, 314
shut down, 316
signal cable connections, 344
solvent mixture equilibration, 322
solvent suppression problems, 321
solvent suppression setup, 317
solvent suppression, retrieving parameters for,
317
transfer tube volume, 341
WET shapes, 322
writing protocols, 363
VAST data sets, examples of plots
96 1D spectra plotted using plvast, 328
using a custom display order, 328
vastget, 326, 340
vastglue, 324, 340
vastglue2, 325, 340
versatile automatic sample transport, 311
vertical scale adjustment, 119
vertical temperature gradient, 263
vloc
as used with VAST, 314
Volume button, 124, 128
vortex plug, 263
Vproj (max) button, 117
Vproj (sum), 117
vs parameter, 112
vs2d parameter, 112, 121
VT accessory, 259
VT Acqmeter display, 260
VT controller, 262
VT Controller label, 260
VT controller power, 260
VT controller safety circuits, 264
VT cutoff, 260
VT experiment warning, 26
VT FAILURE message, 265
VT gas flow rate, 263
VT indicator light, 261, 262
VT nitrogen gas flow, 261
VT operation, 259
VT operation with a sample changer, 298
VT regulation light, 265, 265
vtc parameter, 259, 261
vtwait parameter, 263, 265
VXR-4000/Gemini data system, 174
WALTZ decoupling, 173
WALTZ-4 modulation, 183
warnings defined, 25
water eliminated through transverse gradients 1D,
457
water in VT exchanger, 262
water suppression, 75, 87
wave definition string, 233
wave string variables, 239
waveform generation, 230
wavelib directory, 233
wbs parameter, 306
wc parameter, 36, 109
wc2 parameter, 36, 109
weighting values generation, 95
werr parameter, 297, 306
WET
double relay-COSY, 471
double-quantum filtered COSY, 458
LC-NMR, 404
Nuclear Overhauser Effect spectroscopy, 466
PFG absolute-value COSY, 460
PFG Absolute-Value MQF COSY, 465
PFG HMQC, 462
PFG HSQC, 463
pulse width X channel calibration, 469
relay-COSY, 471
TOCSY with water suppression, 474
VAST, 318
WET experiments
solvent suppression, LC-NMR, 409
solvent suppression, VAST, 322
WET shapes
LC-NMR, 409
VAST, 322
Wet Width
LC-NMR, 407
VAST, 320
wet1d macro, 457
WET1D pulse sequence, 457
wetcosy macro, 471
wetdqcosy macro, 458
WETDQCOSY pulse sequence, 458
wetgcosy macro, 460
WETGCOSY pulse sequence, 460
WETGHMQCPS pulse sequence, 462
wetghsqc macro, 463
WETGHSQC pulse sequence, 463
wetgmqcosy macro, 465
WETGMQCOSY pulse sequence, 465
wethmqcps macro, 462
wetnoesy macro, 466
WETNOESY pulse sequence, 466
wetpwxcal macro, 469
WETPWXCAL pulse sequence, 469
WETRELAYH pulse sequence, 471
wettntocsy macro, 474
WETTNTOCSY pulse sequence, 474
wexp parameter, 299, 307
WFG (waveform generator), 371
wft command, 35, 97, 100
wft1d command, 103, 134
wft1da macro, 104
01-999161-00 A0800
VNMR 6.1C User Guide: Liquids NMR
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